GCMS calibration table data, sample AE10517, May 22, 2002

Machine-extracted title · confidence 90%

Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013285–000013308

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library searcn compound Report

Data File : C:\MSDCHEM\1\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Cyclononasiloxane, octadeca... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 33.20 1.71 ug/L 767974 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 78 2 l,l,l,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00/1 59 3 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 32 4 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 32 Abundance Scan 5127 (33.203 min): 10517.D (-5109) (-) m/z 73.10 00.00 73 147 221 5000 355 . ... 4. ( . 1 1 281 429 32.80 33.00 33.20 33.40 33.60 Tr 41 3251, 191, 504 0- * T • r• • ' I ‘ ‘ ‘ ‘ I ' ' m/z 147.10 69.97% mz-> 0 50 100 '150 200 250 300 350 400 450 500 550 600 650 Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429

355 ................ ........................... 5000 281 32.80 33.00 33.20 33.40 33.60 m/z 221.10 52.66% 475 0- ——————— ’ 11 l * • j • ■ 1 TIT Ha—kHin nH651 miz-> 050 100 150 200 250 300 350 400, 450 500 550 600 650 Abundance #26950:1,1,1,5,7,7,7-HeptamethyI-3,3-bis(trimethylsiloxy)... 73 ........ .. 147 32.80 33.00 33.20 33.40 33.60 5000 267 m/z 355.00 31.87%| 355 429 207 ......................... .......... 0 t■■*■i TI i ■ ■ ■ ■ i 1 ■ 1111 i ■ ■ ■' i''' ■ i11 n/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyj)~ 73 32.80 33.00 33.20 33.40 33.60 147 ....................

5000 221 _ WwAWAAo n/z-> 0 MJ 0 104 177. - — ++11ttt1***s1*’’*1*+**14*’II 50 100 150 200250300350400 450 500550600650 32.80 33.00 33.20 33.40 33.60

10517.D 052202.M Wed May 22 11:48:25 2002 Page 15

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