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GCMS analysis results for sample AE10164, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for sample AE10164 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023487–000023501

Folder label: “GCMS X 5/9/02 A 5/13/02

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Scanned page image, NYC-WTC_000023500
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\10164.D Vial: 12 Acq On : 13 May 2002 8:27 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Benzene, 4-bromo-l-chloro-2... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.94 0.40 ug/L 226204 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, 4-bromo-l-chloro-2-(tri... 258 C7H3BrClF3 000445-01-2 9 2 4a,8a-Methanophthalazine-l,4-dic... 260 C13H12N2O4 118643-90-6 9 3 Phenindamine 261 C19H19N 000082-88-2 77 4 Phenindamine 261 C19H19N 000082-88-2/ 7 Abundance Scan 5423 (34.942 min): 10164.D (-5421) (-) m/z 207.00 100100% 207

5000 73 260 281 wpslHshwrnP" 117 130 40 34.60 34.80 35.00 35.20 01 m/z 260.10 60.36%| mfe-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance: #127799: Benzene, 4-bromo-1-chloro-2-(trifluoromethyl)- 260 179 5000 75 34.60 34.80 35.00 35.20 144 m/z 281.00 41.62%| 37 50 62 89 109 125 2 223 241 159 0 II 11 1 1 -Hth—4H——7 ' -P 191210 U...1, mlz-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 #94575: 4a,8a-Methanophthalazine-1,4-dicarboxylic acid, di... 141 260 n 116 34.60 34.80 35.00 35.20 5000 59 m/z 73.20 39.46%| 89 228 , 102 129 187 201

n/z-> 01 i ■ ■ I20 44 — 40 l 60 80 I I 1 1 1 1 1 4 I 1,,245., 1 । 1 1 * > । II * *.............. 100 120 140 160 180 200 220 240 260 280 Abundance #94655: Phenindamine 260 4 34.60 34.80 35.00 35.20 m/z 261.10 35.86%|

5000

42 57 76 94 115 135148 166 . 184 202 947 । 0 44.4 229 244 1 1 ■ i ' ■ 1 ' i ■ ■ ‘ ' i ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 | 34.60 34.80 35.00 35.20

10164.D 050102.M Tue May 14 11:42:14 2002 Page 9

NYC-WTC_000023500

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NYC-WTC_000023500Source: NYC Law Department, mirrored locally

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