GCMS analysis results for sample AE11383, May 22 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11382.D Vial: 9 Acq On : 17 May 2002 7:18 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 4-Bromo-2-trifluoromethylph... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

36.83 0.22 ug/L 176595 Perylene-d12 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Bromo-2-trifluoromethylphenyl ... 281 C8H3BrF3NSI 1000134-47-9 7 2 Acridine, 4,5,9-trichloro- 281 C13H6C13N 1000162-77-77 3 lH-Benzo[d]imidazole, 5-methoxy 148 C8H8N2O 1000197-63/7 5 4 Benzoic acid, 3-(dimethylamino)-... 283 C17H17NO3 055153-17-8 5 Abundance Scan 5744 (36.829 min): 11382.D (-5742) (-) m/z 96.10 100.00% 95 191 283 148

M 1 4 v 5000

221 111 11 1 i 1 ■ 429 36.40 36.60 36.80 37.00 37.20 0-T 40 I l i m/z 191.10 89.12% m/z-> 0 50 100 150 200 250 300 350 400 Abundance #97375:4-Bromo-2-trifluoromethylphenyl isothiocyanate 281 /

5000 202 1 ■ 1 i 1 1 TT^ 75 144 36.40 36.60 36.80 37.00 37.20

i 50 m/z 283.00 83.67% 4 264014/4444*101 182 225 - , , 0 J 1 123 4lpsl I, । Il I1 249 . 1, /z-> o 50 100 150 200 250 . 300 350 400 Abundance #97376: Acridine, 4,5,9-trichldro- 281 i ' 1 1 ' I ' ‘ ■ ■ i ■ ■ 36.40 36.60 36.80 37.00 37.20 5000 m/Z 148.00 75.85% 211 _ 123 175 246

/z—> O—T 0 40,74.23, 1149, 1, A 50 100 150 200 250 M1 300 T 350 400 Abundance #66524:1 H-Benzo[d]imidazole, 5-methoxy 1 1 i ■ 1 T' 1 ' ' I ' 1 1 1 i 1 ' 148 36.40 36.60 36.80 37.00 37.20 m/z 280.90 68.03%

5000

0 52 78 1 , ,4 +14,4 +1l, 105

T-t—r Mp"h I 1 1 1 ' I ' ' n/z-> 0 50 100 150 200 250 300 350 400 36.40 36.60 36.80 37.00 37.20

11382.D 050102.M Tue May 21 11:54:26 2002 Page 11

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