GCMS analysis results for sample AE11383, May 22 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\051702\11382.D Vial: 9 Acq'On : 17 May 2002 7:18 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

36.79 0.36 ug/L 286442 Perylene-d12 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4,5,7-tetrasilaoctan ... 294 C10H30O2S14 004342-25-0 47/ 2 1,3-Benzodioxole, 5-[3-acetamino... 221 C12H15NO3 1000124-33-0 12 3 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9/9 4 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-/ 9 Abundance Scan 5738 (36.793 min): 11382.D (-5710) (-) m/z 221.10 100.00%

5000

44 — 73 147

I 221

191 L 281

1 .1, 355 429 A ' i 1 ■ ■ ' i 1 1 • ’ i ■ ■ 36.40 36.60 36.80 37.00 37.20 ' ‘ i ■ ‘

A o1 TI m/z 147.00 85.51% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 221

73 5000 ■ ■ i ■ ■ 36.40 36.60 36.80 37.00 37.20 191 m/ z 73.00 63.89% 117 279 0- 45 T h 249 | 1 i r 1 । ■ i ■ ■ ■ ' i 1 ' 1 ' i ‘ 1 ■ ■ i ■ TI m/z-> 50 100 150 200 250 300 350 400 450 Abundance #87894:1,3-Benzodioxole, 5-[3-acetaminopropyl]- 221 135 162 36.40 36.60 36.80 37.00 37.20 43 73 5000 m/z 207.00 36.99% 104 vhwoAupawe"NMoby" n/z-> 0- 144,41,41,92,).. 50 100 150 200 250 ■ I ‘ ■ i ■ ' ' ■ i ' ' 1 ■ 1 1 ' ' 1 I 300 350 400 450 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... 73 36.40 36.60 36.80 37.00 37.20 m/z 3 55.00 36.11%

5000 207

M 281 355 X 133

/z—> 0 50 + 103,1,4,17741, 253 L [ 327 | 377399 429 489 100 250 150 300 200350 400 ■ i ' ‘ 450 ' f—■' 1 1 ' i ' 1 1 ki-' ' ■ r-k1 i r ' i ' ' 1 1 i ' 1 ‘ ' i ' 1 36.40 36.60 36.80 37.00 37.20

11382.D 050102.M Tue May 21 11:54:26 2002 Page 10

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