GCMS analysis results for sample AE11383, May 22 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11382.D Vial: 9 Acq On : 17 May 2002 7:18 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Anthracene-diO - Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.47 ug/L 612857 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dl0- 001719-06-8 87 188 C14D10 2 2,2,9,9-Tetramethyldec-5-ene-3,7... 102745-35-7 40 188 C14H20 3 3-Amino-4-methyl-6-methoxyquinoline 1000213-71-3 40 188 C11H12N2O 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3409 (23.109 min): 11382.D (-3401) (-) m/z 188.10 100.00% 188

5000

— 80 94 22.80 23.00 23.20 23.40 132 146 158 43 52 0 ' i " 111'1" i " " i'''111111 66 I i --H TTITTTTIWTPTTTTTHTTTHTTTTTTT —H ।11 ■' । m/ z 94.05 16.67% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 .......................... ............ 22.80 23.00 23.20 23.40 m/z 189.10 14.73% 17 30 42 52 66 0 80 J 94 J 108 118 132 146 1 60 1. 170179 ,h 0- 11 n j j । 11 11 [ i rn [ I 11 । [ I 11 11 11 11 । 11 11 | i 11 I [ I 11 111 r j 11 11 11 11 । 11 I'l'i t 11 i 11 11 11 rl |‘i i । i p r 11 |'I’l l I'] । 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79801: 2,2,9,9-Tetramethyldec-5-ene-3,7-diyne 188 173 41 131 143 1 1 i 1 1 1 1 1 1 1 1 ■ i ' 1 1 1 i ■ ■ ■ ■ i 22.80 23.00 23.20 23.40 91 5000 77 158 m/z 184.05 11.19% 57 119 27 67 105

mfe-> 0 Ip+Hl+)4 4 +7H Tu — +— 1—44+ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/ z 80.10 10.98% 145 5000

117 41 130 51 159 173 63 77 89 102 0 TPP---------++-++---++---++---+------- '■4 ■" i-'1'" i'' II.. /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11382.D 050102.M Tue May 21 11:54:25 2002 Page 9

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