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GCMS analysis results for sample AE11383, May 22 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE11383 conducted on May 22, 2002.

NYC-WTC_000025145–000025162

Folder label: “GCMS X 5/15/02 A 5/17/02

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Scanned page image, NYC-WTC_000025158
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11382.D Vial: 9 Acg On : 17 May 2002 7:18 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 5 1,5-Naphthalenedithiole Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

22.58 0.30 ug/L 392022 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 50 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42A 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 1y) Abundance Scan 3319 (22.580 min): 11382.D (-3312) (-) m/z 192.10 100.00% 192

5000

— 52 42 vn 70 82 96 146 160 | .....n... a. 22.20 22.40 22.60 22.80 23.00 0 11————] Hl m/z 191.10 22.99% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950:1,5-Naphthalenedithiole 192

5000 159 22.20 22.40 22.60 22.80 23.00 115 128 m/z 193.10 14.49% 40 57 69 79 96 106 147 177 0- —TH 44— m/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 - 161 22.20 22.40 22.60 22.80 23.00 5000 m/ Z 96.10 13.83% 77 121 149 177 91 103 52 64 138 0 - T’l — ITT mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- TI TT 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 13.12%

'5000

_ 96 155 , 29 39 51 63 74 83 1 115 126 139 152 0 1 I ‘ 1 " I 1 1 1 rl 1 " 1 P1 " | ''m , | i ri , fl'. .T| 1 " rp', . . । , r, . । , . , . | । 176 , q , . . , p . . . | .'l1, 1 | , rlu | . l i’l 11—3 0 m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

11382.D 050102.M Tue May 21 11:54:23 2002 Page 8

NYC-WTC_000025158

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NYC-WTC_000025158Source: NYC Law Department, mirrored locally

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