GCMS analysis results, sample AE12534, June 2002

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Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014578–000014606

Folder label: “GCMS X 5/28/02 A 5/29/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12534.D Vial: 25 Acq On : 30 May 2002 5:37 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ******* * * ************************************************************ Peak Number 12 1,5-Naphthalenedithiole Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.25 ug/L 238781 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 50 2 Phenanthrene , 3-methyl- 192 C15H12 000832-71-3 42 3 Phenant hrene, 1-methyl- 192 C15H12 000832-69-9 36 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 36 Abundance Scan 3311 (22.533 min): 12534.D (-3304) (-) m/z 192.10 100.00% 192

5000

42 51 70 82 96 146 j 160 .... n..... 22.20 22.40 22.60 22.80 O' —pmpHmmmmmmmpmmpp +pe m/z 191.10 19.64%I miz-> 20 30 40 50 60 70 80 90 100110120130140150160 170180190 200 Abundance #80950:1,5-Naphthalenedithiole 192

5000 159 22.20 22.40 22.60 22.80 115 128 m/z 96.00 15.27% 40 57 69 79 96 147 177 0: । j 11111 i‘i. rel । ['. rh rirrlyevpfrrr - 11* “■« I “ i-r-pT niz-> 20 30 40 50 60 70 80 90 100 110120 130140 150 160 170 180190 200 Abundance #81041: Phenanthrene, 3-methyl- 192

22.20 22.40 22.60 22.80 5000 m/z 146.10 15.26%|

27 39 51 63 82 l 96 115 126 139 152 19 176 cE 0 11..., ।.... ।.,., ।.... । r.,. ।. ri i |T, rl ], 1'111.... ।, n > 1111, ।! 1 r’l < < । ■ "hi 11 g"’t" 11 n l'i 111 "’l 1 m/z-> 20 30 40 50 60 70 80 90 100 110120 130140 150160 170 180190 200 Abundance #125856: Phenanthrene, 1-methyl- 192 22.20 22.40 22.60 22.80 m/z 193.00 12.34%| 5000-

96 ,

/z—> 27 39 51 63 82 J 115 126 139 152 100 178 , L 0- 11.... ।.... j ,,.. ]... 111'1..,. ri । rl’s rl 1 ll i| । > 111 rr. 111, ।, 1111 i-j uh |T > । > । t’t’ 1111 I 11 i'i'I ‘11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 - 22.20 22.40 22.60 22.80

12534.D 052202.M Mon Jun 03 11:46:46 2002 Page 15

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