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GCMS analysis results for sample AE12162, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12162 conducted on June 5, 2002.

NYC-WTC_000013643–000013665

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 Phenanthrene, 1-methyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

22.54 0.24 ug/L 221131 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 53 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 Abundance Scan 3312 (22.539 min): 12162.D (-3304) (-) m/z 192.10 100.00% 19 2

5000 ........ / , ...... no 96 146 160 22.20 22.40 22.60 22.80 40 49 70 82 | | | 0 I 11 i i > 11 > Il | 1 I | | | ri | 1 11 i I 111 > । I I I i | | I I | । । ।j .. I . ।... I|....t।. hpr m/z 191.00 19.33% miz-> 20 30 40 50 60 70 - 80 90 100110 120 130 140 150 160 170 180 190 200 Abundance #125856: Phenanthrene, 1-methyl- 1912

5000 22.20 22.40 22.60 22.80 m/z 193.10 14.16% 27 39 51 63 82 115 126 139 152 165 178 . | 0- 1111'i 11111‘| ri rrpi i rrp’i . 'I'] IIti |'li rlpu II 1’1 .. i . Fom TTTrp . 111'| 11 i i [*I. i। i'l 11 [..!'! । >. .'I) I. > j <. miz-> : 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance! #125842: Phenanthrene, 2-methyl- 192 ■ ■ i ■ ‘ ‘ i ' ' i 1 ■ ' ■ i ■ ‘ ' i 22.20 22.40 22.60 22.80 5000 m/z 146.10 13.33%

96 27 39 115 126 139 152 165 176 51 63 82 J 0- (। TIHptt | I 1 1 I | 1 I I l'| I I I I fl I I I | I'l . I |'l IT. fl', rli .TI l( J + niz-> 2030405060 70 8090 100110120 130140 150160 170180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 Sm 22.20 22.40 22.60 22.80 m/z 96.00 12.20% 5000

96 165 । , 29 39 51 63 74 83 l ‘ 115 126 139 152 ,| 176 J, | 0 TPWTTTTTTTTTUTTTTTTITTLPTTTTTTTTTTHTT ■' I ■ ■ ■ ■ i ■ ■ ■ ■ i • ' I ' ' ' ' I ' ' i /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

12162.D 052202.M Wed May 29 09:55:13 2002 Page 13

NYC-WTC_000013660

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NYC-WTC_000013660Source: NYC Law Department, mirrored locally

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