GCMS blank analysis results for sample AE11379, May 21, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\0515LB.D Vial: 16 Acq On : 18 May 2002 1:49 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 7-(4-Bromophenyl) -10,10-dim... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

33.14 1.19 ug/L 806859 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 7-(4-Bromophenyl)-10,10-dimethyl... 429 C25H20BrNO 1000149-13-0 4 2 2-Methylidenehydrazono-3-methyl-... 191 C9H9N3S 1000147-35-2 9 3 1,3-Butadiene, pentachloro- 224 C4HC15 055880-77-8 / 4 1-(3-Cyano-4,5,6,7-tetrahydro-2-... 427 C21H21N303S2 1000225-91-/ 9 Abundance Scan 5116 (33.139 min): 0515LB.D (-5114) (-) m/z 191.00 100/00%| 191 221 49 355 431 149 5000 74 ‘ d 1 I l 1 ■ ■ ■ 1’’ ‘ ’ [ 1tt 267 295 0- I J... ... I . I I ||... i 1 ■ ■ ■ i ' 1 1 1 i 1 ' ■ ■ i 1 ■ ■ ■ i ■ 1 ■ 1 i ’ nk' i ■ diTdB 32.80 33.00 33.20 33.40 m/ Z 2 0 5.10 92.48%|

A miz-> 50 100 150 200 250 300 350 400 Abundance #106191: 7-(4-Bromophenyl)-10,10-dimethyl-8,9,10,11 -tetrah... 4:11

233 294 5000 .... 11 ....... 265 375 32.80 33.00 33.20 33.40 400 m/z 221.10 92.48% 350 0- I m/z-> 50 100 150 200 250 300 350 400 Abundance #80614: 2-Methylidenehydrazono-3-methyl-2,3-dihydrobenzoth... 191

32.80 33.00 33.20 33.40 5000 m/ z 2 08.00 71.68%I 149 109 69

m/z-> 0- 42 ila 1) I TT ' 50 I 100 150 ' 200 r ‘ 250 300 350 400 IM,./' Abundance #80672:1,3-Butadiene, pentachloro- 191 32.80 33.00 33.20 33.40 m/ z 49.00 68.14%

5000 84 226 49 119 154

0 25/ — mfe-> 50 100 150 200 250 300 350 400 32.80 33.00 33.20 33.40

0515LB.D 050102.M Tue May 21 11:58:22 2002 Page 10

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