GCMS sample analysis results, AE11901, June 4, 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11901.D Vial: 8 Acq On : 22 May 2002 7:31 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 1,3-Butadiene, pentachloro- Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 36.67 0.42 ug/L 194754 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Butadiene, pentachloro- 224 C4HC15 055880-77-8 9 2 5-Methyl-2-p-methoxyphenylimino-... 222 C11H14N2OS 075220-49-4/9 3 2-(2-Hydroxyethylamino)-4,6-dime... 222 C11H14N2OS 068720-60-5 7 4 2,3-Dicyano-5,6-diphenylpyrazine 282 C18H10N4 052197-23-6 7 Abundance Scan 5718 (36.676 min): 11901.D (-5712) (-) m/z 222.10 0.00% 191 222 207 281 73 5000 49

36,40 3660 36:80 37.00 0-1inn 11 > A ■ 111 TTT ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ • ■ i ■ ■1 ■ i ■ ■ ■ ■ i ■ ’t111’171T1"1’’11113 m/z 190.90 94.17% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance

nukuitkunshi #80672:1,3-Butadiene, pentachloro- 191

5000 84 226 49 119 154 36.40 36.60 36.80 37.00 37 m/z 280.90 69.17% ___ 0- ’I 24 4. 1 । I । + 4 1 f i* i J 4V "i141ri 1166. 1_____ Ill,........................ TT—n 11 1111+141114111 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #88160:5-Methyl-2-p-methoxyphenylimino-1,3-thiazolidine 222

36.40 36.60 36.80 37.00 5000 207 m/z 281.90 67.92% 134148 41 63 77 91 165 180 oV """"""""""" , m—AP—Mya— :14 । 108, T, —- nz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #80660:2-(2-Hydroxyethylamino)-4,6-dimethylbenzothiazole 178191 36,40 36,60 36.80 37.00 222 m/z 207.00 66.67% 5000 164 45 65 77 91 103 121 136148 /z-> 0- q 1.129 20 40 60 80 100 120 140 160 180 200 220 240 260 280 ‘ I 1 ■ ■ • i ‘ ‘ ‘ ‘ i 1 ■ ■ • i ‘ ‘

36.40 36.60 36.80 37.00

11901.D 052202.M Tue May 28 12:05:53 2002 Page 21

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