GCMS analysis results for sample AE09569, May 2002

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Data File : C:\MSDCHEM\1\DATA\050902 \9569.D Vial: 24 Acq On : 10 May 2002 10:51 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Hexasiloxane, 1,1,3,3,5,5,7... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

37.77 0.24 ug/L 237364 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexasiloxane, 1,1,3,3,5,5,7,7,9,... 430 C12H3805Si6 000995-82-4 12 2 1-Benzopyrylium, 2-phenyl- 207 C15H110 014051-53-7 9 3 2-Methyl-6-(5-methyl-2-thiazolin... 207 C10H13N3S 1000225-39-3 9 4 Pyrazolo[1,5-a]pyridine, 3-methy... 208 C14H12N2 017408-32-1 9 Abundance Scan 5905 (37.774 min): 9569.D (-5897) (-) m/z 281.05 100. 00% 281

5000 40 73

133 207

356 429 wwhkA/yapottk 37 40 37.60 37.80 38.00 38.20 0- b m/z 73.10 77.80% m/z-> 50 100 150 200 250 300 350 400 Abundance #27715: Hexasiloxane, 1,1,3.3,5,5,7,7,9,9,11,11-dodecamethyl- 73

5000 281 207 37 40 37.60 37.80 38.00 38.20 133 m/z 207.00 75.85%

n/z-> 0- 4 50 103 100 J 153 177 s 1 234253 150 200 1 r1 1 250 300 1^309 341 N........... 415 350 400 AwwyMvHnyvM Abundance #84871:1 -Benzopyrylium, 2-phenyl- 207 37.40 37.60 37.80 38.00 38.20 5000 m/z 221.10 59.51% 36 131 178

01 L155.,1192A----—— [ 'l l 152 ‘ 1 r I 1 ' 1 1 1 ' ' i ■ 1 ■ ' i ' .......... ........................................... n/z-> 50 100 150 200 250 300 350 400 Abundance #84743: 2-Methyl-6-(5-methyl-2-thiazolin-2-ylamino)pyridine 207 37.40 37.60 37.80 38.00 38.20 93 165 m/z 133.00 50.49% 65 119 5000 39 A M

m/z-> 0 50 100 18. 185 — ................... ........... 150 200 250 300 350 400 ' । ■1 37.40 37.60 37.80 38.00 38.20

9569.D 050102.M Mon May 13 11:45:36 2002 Page 9

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