GCMS analysis results for sample AE09569, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\050902\9569.D Vial: 24 Acq On : 10 May 2002 10:51 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 1,2-Benzenedicarboxylic aci... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.38 0.35 ug/L 469606 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 74 2 Bis(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 72 3 Bis(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 64 4 Bis (2-ethylhexyl) phthalate 390 C24H3804 . 000117-81-7 64 Abundance Scan 4816 (31.376 min): 9569.D (-4809) (-) m/z 149.10 100.00% 149

5000 227 57 167 43 71 113 207 279 31.00 31.20 31,40 31.60 31.80 O-T 'p^p1....... Il..... ’L —PPPTP m/ z 22 7.20 43.40% ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #67063:1,2-Benzenedicarboxylic acid, diisooctyl ester 149

5000 57 167 31.00 31.20 31.40 31.60 31.80 41 71 m/z 167.00 37.82% 104 279 0 ।l + kA ., 11.132 ‘ P 11' ' 1 1 p p '11'11' r ■ ■ ■ r r ■ ■ i ■ ■ ■11 11 ‘ ‘ i' •'' I ■' ■ ■ i' ■'' i'1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #66784: Bis(2-ethylhexyl) phthalate 149 , MAA . ....... 31.00 31.20 31.40 31.60 31.80 5000 m/z 57.10 33.67% 57 167 43 71 113

n/z-> 20 O-T — 40 60 ++93132 4 80 279 1 " I'' ■ ‘ i1 ■' ■ i ■''' i ■'111' ■ “ I'1'' i' " ' i " 100 120 140 160 180 200 220 240 260 280 300 320 naniiiZ’hunu Abundance #123452: Bis(2-ethylhexyl) phthalate 149 31.00 31.20 31.40 31.60 31.80 m/ z 70.10 23.15%

5000 57 167 43 71 113 0 —— 193 .1132 1 p 11-1-11' । i' । p 1111i ■ ■ ■1 p " i 193209 1 ■ ■ i ■' ■ ■ i 261 279 327 ■ i1'111 ‘'1' I' ■ ■ ■ i' ■'' i ■ ■ ' i 1 ■ ■ ' i ■ ’ I’ m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 31.00 31.20 31.40 31.60 31.80

9569.D 050102.M Mon May 13 11:45:36 2002 Page 8

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