GCMS sample analysis results, AE11800, June 3, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11800.D vial: 7 Acq On : 22 May 2002 6:43 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan 7 Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 Pyridine, 1,2,3,6-tetrahydr... Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 39.55 0.33 ug/L 134408 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pyridine, 1,2,3,6-tetrahydro-l-m... 207 C12H14C1N 005048-08-8 9 2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 9 3 1-Cyclohexen, l-cyano-4-isoprope... 147 C10H13N 1000126-45-8 5 4 1,3-Benzodioxole, 5-[3-acetamino... 221 C12H15NO3 100012433-0 4 Abundance Scan 6208 (39.555 min): 11800.D (-6190) (-) m/z 221.10 100.00% 147 Z!1 73

5000 96 281 355 40 429 39.20 39.40 39.60 39.80 — 0- m/z 147.00 90.85% niz-> 50 100 150 200 250 300 350 400 Abundance #84703: Pyridine, 1,2,3,6-tetrahydro-1-methyl-4-[4-chIorop... 42 207

5000- 96 0)1.. 1 39.20 39.40 39.60 39.80 m/z 73.10 67.04% 0 t i LuLMll ,4+168188, miz-> 50 100 150 200 250 300 350 400 Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 73 147 281 39.20 39.40 39.60 39.80 5000 m/z 207.00 50.28%

369 45 0- ' , 44., | 177 .227226 249 L; 310 341 } 95 117 Tr ----- niz-> 50 100 150 200 250 300 350 400 Abundance #65824: 1-Cyclohexen, 1-cyano-4-isopropenyl- 1 • । ■ ■ ■ • । ■ ■ ■ • । ‘ । ■ ■ ■ ■ ।

68 147 39,20 39.40 39.60 39.80 m/z96.10 45.77% 41 5000 96

m/z—> 0- Mta 50 100 ___________________ ______ ._______________ 11d/dTT//2/1////0/1///1/dok////////d/".k/o 150 200 250 300 350 400 A

39.20 39.40 39.60 39.80 h

11800.D 052202.M Tue May 28 12:04:50 2002 Page 22

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