GCMS scan data for sample AE11420, May 2002

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Data File : C:\MSDCHEM\1\DATA\052002\11420.D Vial: 10 Acq On : 20 May 2002 8:37 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 2-(2,6,6-Trimethylcyclohex-... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

34.35 0.30 ug/L 258709 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-(2,6,6-Trimethylcyclohex-1-eny... 222 C14H2202 1000185-64-1 35 2 Trisiloxane, 1,1,1,5,5,5 -hexamet... 384 C12H3604Si5 003555-47-3 27 3 3,6-Dioxa-2,4,5,7-tetrasilaoctan ... 294 C10H3002Si4 004342-25-0 25 4 Mercaptoacetic acid, bis(trimeth. .. 236 C8H2002SSi2 006398-62-5 12 Abundance Scan 5323 (34.355 min): 11420.D (-5316) (-) m/z 73.10 /100.00% 73 147

221 5000 281 355 429 ■ i 1 1 AillAni MW M 49 34.00 34.20 34.40 34.60 I J.......... Il ll , I I I ll..... 0- I 19l TL1 ' i ■ 1 1 ' i — ' m/z 147.10 90.59% m/z—> 50 100 150 200 250 300 350 400 Abundance #66034: 2-(2,6,6-Trimethylcyclohex-1 -enyl)cyclopropanecarb... 147

107 .................... ,.................... A, 5000 — 207 175 34.00 34.20 34.40 34.60 41 79 rn/z 221.10 63.08% 0- LQ1 „L. y. 2 hil 1 . r 1 1 ' 1 ' । 1 226 1 ' । ■ ' ' ■ । 1 ' ' । । । ‘ । । miz-> 50 100 150 200 250 300 350 400 Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 73 147 281 34.00 34.20 34.40 34.60 5000 m/z 206.95 39.53%

n/z-> Abundance 0- 45 - T-i95I 117 50 100 1* 1 177 207226 249 I r . J p-min r-t 1"i 11 1‘1| 150 200 250 ,1 310 341 | 300 350 #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7 -- 147 22!1 400 369

A34.00 34.20 34.40 34.60 m/z 281.00 32.87% 73 5000 191 117 279 0 45 T-- ' r 1 1 1' 1 1 ' A I., 1 , 249 . +................... AAMQA4 m/z-> 50 100 150 200 250 300 350 400 34.00 34.20 34.40 34.60

11420.D 050102.M Thu May 23 14:07:11 2002 Page 10

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