GCMS sample analysis results, AE11800, June 3, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.

NYC-WTC_000012823–000012851

Folder label: “GCMS X 5-21-02 A 5-22-02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11800.D vial: 7 Acq On : 22 May 2002 6:43 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L *********************************************************** *** * * * **** Peak Number 20 5H-Pyrido[1,2-c]pyrrolo[1,2... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 39.60 0.46 ug/L 188081 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual .1 5H-Pyrido[l,2-c]pyrrolo[l,2-a]py. .. 222 C14H26N2 114530-37-9 9 2 3-(6-Bromohexyl)-2,4,10-trioxaad... 304 C13H21BrO3 088784-99-0 9 3 4-Benzofurazanamine, 7-nitro-n-p... 222 C9H10N4O3 054517-98-5 7 4 Perhydro-htx-2-one, 2-depentyl-,... 281 C16H27NO3 1000126-27-9 7 Abundance Scan 6215 (39.596 min): 11800.D (-6212) (-) m/z 96.00 400.00% 73 95 193 209 281 369 'J 5000

V 44 39 20 39.40 39.60 39.80 0A— I ‘1 “ i1 ■ ■' i “ ■ ‘ i •" ' i “ “ i" ■ ‘ i “ “ i “ “ i ‘ “ i “ ‘ ‘ i “ “ i ■ ■ “ i ■' “ i “ “ i m/z 73.10 98.31% miz-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance> #81222:5H-Pyrido[1,2-c]pyrrolo[1,2-a]pyrimidine, decahydr... 193 96 221 152 5000 41 39.20 39.40 39.60 39.80 70 123 m/z 193.10 79.75%

OTmp I ■ “ ■ I • •, ■ l ■■ ‘ ■ l ■1 ■ '" I ' i • ■ i • ■' ■ i ■1" i “ ■ • I ■1 ‘ ■ i ■ ■' ■ i “ ■ i' • ■ ■ I m/z—> 20 40 60 80 100 120 140 1«) 180 200 220 240 260 280 300 320 340 360 Abundance #41809:3-(6-Bromohexyl)-2,4,10-trioxaadamantane 96 191 39.20 39.40 39.60 _________ 39.80 . 5000 55 m/z 83.90 73.84%

044 27 79 fr44—4+ .121138,29 TPIm 156 260276 394 T’’h finr, .1. r,. 1* II’TI’ H 11 225 k/ AAh wN AM A tnfz~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #81409:4-Benzofurazanamine, 7-nitro-n-propyl- 1 i' ■ ■ ■ I 117 193 222 39.20 39.40 39.60 39.80 m/z 209.10 67.09% 5000 43 I A

27 76 92 044HRR.# +4r* 145163 itr rrh poaoponsyannagmenagoma m re , .| i।, III] III, fill) IIIH lllll. mfz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 39.20 39.40 39.60 39.80

11800.D 052202.M Tue May 28 12:04:52 2002 Page 23

NYC-WTC_000012850

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GCMS sample analysis results, AE11907, June 4, 2002 · Box DEP Box 15

NYC-WTC_000012989

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.

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