GCMS analysis results for sample AE11418, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052002\11418.D Vial: 8 Acq On : 20 May 2002 6:59 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 8 1H,3H-Pyrrolo[1,2-c][1,3,2]... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

34.87 0.26 ug/L 182161 Perylene-dl2 34.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1H,3H-Pyrrolo[1,2-c] [1,3,2]oxaza... 207 C11H14NOP 111002-64-3 9 2 4-Fluorothiophenol 128 C6H5FS 000371-42-6 7 3 1,2-Benzenediol, 3-fluoro- 128 C6H5FO2 000363-52-0 5 4 2,5-Diphenyl-3(H)-pyrrol-3-one, ... 262 C17H14N2O 075096-72-9 5 Abundance Scan 5411 (34.872 min): 11418.D (-5410) (-) m/z 128.00 00.00% 128 116 44 207 256 5000 232

84 96 34.60 34.80 35.00 35.20

m/z-> 01 ■ ■ I 1 1 ' | ' " . , । . i i | I . i I | ' 1 , . 20 40 60 80 100 120 ■ r ■ ■ ' ■ i ‘ 140 160 ' 1 I ■ 180 -P 200 220 240 260 m/z 116.30 63.64%

Abundance #58994:1 H,3H-Pyrrolo[1,2-c][1,3,2]oxazaphosphole, tetrahy... 130 207 177 ,........................ 5000 55 34.60 34.80 35.00 35.20 83 m/ z 130.00 54.55% 27 39 107

m/z-> 0- . 1, J 14zululy, 95,4 + +++,164.4,4 20 40 60 80) 100 120 140 160 180 149 . .192 +r 200 220 240 260 Abundance #121775: 4-Fluorothiophenol 128 34.60 34.80 35.00 35.20 5000 108 m/z 207.00 51.07% 84 „ 45 5/ 69 96 0- 111 Aadlt .4 4 - li ........................ AAMuLAoruhi rn/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #57985:1,2-Benzenediol, 3-fluoro- 128 34.60 34.80 35.00 35.20 m/ z 44.10 50.80%| 5000 52 80 . 26 39 J 64 02 108 O—r -1"! ."'I I-A' rljpprI" M 0* , IT ' 1 i ' ' ■ ■ i ■ ■ 1 ■ i ‘ ' i ' ' ' ■ i 1 1 ' 1 I ' 1 1 ' I 1 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20

11418.D 050102.M Thu May 23 10:46:15 2002 Page 11

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