GCMS analysis results for unknown compounds, sample AE09093, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\9093 .D Vial: 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 5H-Pyrido[1,2-c]pyrrolo[1,2... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 33.12 0.31 ug/L 240683 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5H-Pyrido[l,2-c]pyrrolo[l,2-a]py... 222 C14H26N2 114530-37-9 18 2 2-Buten-1-one, 1,3-diphenyl- 222 C16H140 000495-45-4 9/ 3 2-Styryl-1,3-dithiane 222 C12H14S2 1000146-50-4 9 4 2-Amino-2-oxo-acetic acid, N- [3, . . . 221 C12H15NO3 1000127-85-3 9 Abundance Scan 5113 (33.121 min): 9093.D (-5107) (-) m/z 73.00 100.00% 73 221 147 429 5000 96 356 36 295 m A, . Al A _ i । i — l-i r—। _i L _ i — i i — 32.80 33.00 33.20 33.40 01 Ui m/z 221.10 72.82% Tl/Z—> 50 100 150 200 250 300 350 400 Abundance #126950: 5H-Pyrido[1,2-c]pyrrolo[1,2-a]pyrimidine, decahyd... 193 221

152 5000 96 I 1 1 I ' ' 1 1 I ' ' ' ’ I ' 1 1 1 I

A. 1 ■ i 1 32.80 33.00 33.20 33.40 41 70 1 m/z 147.10 51.26%

m/z--> 0- I 50 1.11731/,100 150 200 T*-p-r—r-T-r—r-r-r—r—t—i 250 300 11*‘I 350 400 Abundance #87849: 2-Buten-1-one, 1,3-diphenyl- 77 221 115 51 32.80 33.00 33.20 33.40 5000 m/z 42 9.00 50.68% 145

m/z-> 0- 27 —L | JUL i f r ’ 50 100 1178222— 150 200 250 1 300 i 1 1 1 1 350 i ■ ■ 1 1 400 1 1

Abundance #66301: 2-Styryl-1,3-dithiane 1 ' i 1 1 1 1 । ' 1 1 । 1 1 1 1 । 1 1 1 1 । 147 32.80 33.00 33.20 33.40 222 m/z95.90 43.11% 5000 115

45 72 189 0 ill "r L Ih l TL' I । | । । i r । I l I | I i i i [ I | l 1 1 1 i ' 1 ■ i ■ TTf m/z-> 50 100 150 200 250 300 350 400 32.80 33.00 33.20 33.40

9093.D 050102.M Thu May 09 13:33:34 2002 Page 12

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