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GCMS analysis results for unknown compounds, sample AE09093, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE09093 on May 10, 2002.

NYC-WTC_000044902–000044925

Folder label: “GCMS X 4/30/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\9093 .D Vial: 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 10 D-Lysergic acid monoethylamide Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

33.19 0.64 ug/L 502854 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 D-Lysergic acid monoethylamide 295 C18H21N3O 000478-99-9 14 2 2-Propen-1-one, 3-(4-methylpheny. . . 222 C16H140 004224-87-"/ 9 3 4-(3-Hydroxy-2,6,6-trimethylcycl . . . 222 C14H2202 097306-57/5 9 070231-36-6 5

A 4 2-Isopropyl-6-phenylnicotinonitrile 222 C15H14N2 Abundance Scan 5124 (33.186 min): 9093.D (-5117) (-) m/z 147.05 100.00% 147

207 295 5000 84 355 429 1 1 ■ 1 1 ' 1 1 1 40 32.80 33.00 33.20 33.40 33.60 01 — Tl Tl 1 1 1 LiI1 m/z 207.00 58.11% m/z-> 50 100 150 200 250 300 350 400 Abundance #98911: D-Lysergic acid monoethylamide 205 uaW""yhyok 221 5000 > । 1 1 kl । 1 1 I I | । 1 r~i । i-1 1 1 । 1 1 181 32.80 33.00 33.20 33.40 33.60 154 m/z 221.00 56.31%

0- i I 57 — JI I , UU 112 itI I 1• I Ii 1 , | 4 1 | , 22 Tl 1 fl T ' m/z-> 50 100 150 200 250 300 350 400 Abundance #84905: 2-Propen-1-one, 3-(4-methylphenyl)-1 -phenyl- 207

32.80 33.00 33.20 33.40 33.60 5000 145 m/z 295.00 52.70% 105 51 179

m/z-> 01 11Z7 50 100 lh । . 7 1 1 1 14150 1 1 * 200 Tfl 250 1 1 1 300 1 T-1 350 Tl 1 400 Abundance #84761:4-(3-Hydroxy-2,6,6-trimethylcyclohex-1-enyl)pent-3... 1 1 1 1 ' ' 1 1 1 1 1 1 1 1 1 1 43 123 207 32.80 33.00 33.20 33.40 33.60 m/z 83.90 43.54% 148 5000 AAl 69 91

m/z-> 0 I |; I dapls 4 l,l ll 4 j. ulal+ 50 100 , 179 Ji, 226 150 2001 —T ■' ' i 1 250 300 1 l 350 1) 1 400 | 1 1 I • ' 32.80 33.00 33.20 33.40 33.60 TdT Tilt 44

9093.D 050102.M Thu May 09 13:33:35 2002 Page 13

NYC-WTC_000044919

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