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GCMS analysis results for unknown compounds, sample AE09093, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE09093 on May 10, 2002.

NYC-WTC_000044902–000044925

Folder label: “GCMS X 4/30/02 A 5/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\9093.D Vial: 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Naphthalene, 1,2,3,4-tetrah. . . Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

34.97 0.22 ug/L 171955 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Naphthalene, 1,2,3,4-tetrahydro-... 177 C10H11NO2 029809-14-1/9 2 6-Azatetracyclo[6.5.0.01,7.04,11... 187 C12H13NO 056689-39-5 9 3 Methyl(methyl 2,4-di-O-acetyl-3-... 320 C13H20O9 087910-31-4 9 4 1-Cyclohexene, 4-hydroperoxy-1-p... 190 C12H1402 1000142/30-4 9 Abundance Scan 5427 (34.966 min): 9093. D (-5426) (-) m/z 132.80 100.00% „ 133 209 263 116 41 96 5000 L | 1111'111 73 34.60 34.80 35.00 35.20 111 ’ ।' .. ...... I,I... 001] ' 1 I 1 1 m/z 2 09.00 94.53% n/-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #121920: Naphthalene, 1,2,3,4-tetrahydro-5-nitro- 130 91 115 159

5000 177 77 51 m/z 263.10 90.88% __ 143 O-TT TTdd11/1/n/k .‘■r/ , aule , , I I I I I I I I I I I I | I > I I | I r I I | I I I I [ TT

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #58456: 6-Azatetracyclo[6.5.0.01,7.04,11 ]trideca-2,12-dien... 129 I [ r/ i s T I I i | I I I I | I I ! I | T

115 34.60 34.80 35.00 35.20 5000 m/ z 129.10 82.48%

51 -70 91 64 78 I | I . 144 173 m/z-> O-TT 20 40 60 1. . 1 ■ । । v । T [ i । । । । n l [ । । । । । । । । । । ti " i" r [ "i "i i i [ 80 100 120 140 160 180 200 220 240 260 280 tt

Abundance #8629: Methyl(methyl 2,4-di-O-acetyl-3-O-methyl-.alpha.-D-... 1 1 11 43 130 34.60 34.80 35.00 35.20 m/z 116.00 81.02% 75 5000 101 158 59 115 59 I £8 145 । 189 '73 1 1 O- #, lu < #ph, fW1, ,4', —H—44J| T I i i' r | i I t 216229 i | i i i I | ii'< i | i i 261 ■ ■ r" ' ■ । 289 ■ I | ’ i i | | ′′ f |r | I I I I-1 ! 1 | TT

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

9093.D 050102.M Thu May 09 13:33:36 2002 Page 14

NYC-WTC_000044920

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NYC-WTC_000044920Source: NYC Law Department, mirrored locally

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