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GCMS blank analysis results for VOCs, May 9 2002

Machine-extracted title · confidence 100%

Laboratory report of a GC/MS blank run analyzing volatile organic compounds with results below detection limits in May 2002.

NYC-WTC_000045547–000045563

Folder label: “GCMS X 5/3/02 A 5/7/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\0503LB.D Vial: 5 Acq On 7 May 2002 4:24 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L Peak Number 7 Naphthalene, 1,2,3,4-tetrah. . . Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 34.89 0.31 ug/L 284181 Perylene-dl2 34.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Naphthalene, 1,2,3,4-tetrahydro-... 208 C16H16 003018-20-0 9 2 Methane, bromochloro- 128 CH2BrCl 000074-97-5 7 3 Methane, bromochloro- 128 CH2BrCl 000074-97-57 4 Methane, bromochloro- 128 CH2BrCl 000074-97/5 7 Abundance Scan 5414 (34.889 min): 0503LB.D (-5413) (-) m/z 2 08.00 100.00% 40) 208 232 102115 281 .

86 5000 130 259 AAAA,AAAM । MMAAMKYMMMN 34.60 34.80 35.00 35.20 ‘ I • ' ' 1 ' ' I 1 ' 1 1 1 1 i-r । । । । i । i rh । । । r TT] n । । । m । । । r ■ 1 i ' 1 ‘I । I i i t I i rn [i- m/z 40.10 90.23% m/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 #126509: Naphthalene, 1,2,3,4-tetrahydro-1-phenyl- 260 280 wv/MwpnM"M»/ 208 180

5000 130 1 I | । । । । । i l i । i 11 i [ i r 34.60 34.80 35.00 35.20 165 m/z 232.10 91 104 81.11% 77 1.17 / 152 1 I I I I I I I I I I I I I I > I I I II I ] I I I I I TI I I 1 193 " ' ' I ' ' 1 1 I'1 1 ' ' I n-n-p-r m/z->20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #12332: Methane, bromochloro- 49 130 । | ■ ■ ■ ' | 177 I | ! । । । | I I 34.60 34.80 35.00 35.20 5000 m/z 102.10 77.20% 93

j| , 64 , ‘ , . 1' I I I I II I 1 1 I 116 TIT i । । 111717/1 । । । । । । । । । । IT i"i "i i । i i i i ।—i i i i" । i r t i | ’ / i. . i—i—।—!—i—i—i—।—i—r m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #111044: Methane, bromochloro- 49 130 34.60 34.80 35.00 35.20 m/z 281.00 73.29% 5000

1 |" 93 A II I

m/z—> 1435 "‘I 1 1 ’ 1 I ' l +93,, | 20 40 60 64 79 i.. 80) 116 1 ! I > | ■ I । I | P

100 120 ' I 1 1 1 ' 1 1 1 1 ' I 1 ' ' 1 I ' 1 1 1 1 1 1 1 1 I r 1 1 1 1 1 ' 1 1 1 1 ' 140 160 180 200 220 240 260 280 J ih | lli ilh lTf 34.60 34.80 35.00 35.20 LaAliLIL 0503LB.D 050102.M Thu May 09 09:21:15 2002 Page 10

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NYC-WTC_000045560Source: NYC Law Department, mirrored locally

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