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GCMS blank analysis results for VOCs, May 9 2002

Machine-extracted title · confidence 100%

Laboratory report of a GC/MS blank run analyzing volatile organic compounds with results below detection limits in May 2002.

NYC-WTC_000045547–000045563

Folder label: “GCMS X 5/3/02 A 5/7/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\0503LB.D Vial: 5 Acq On 7 May 2002 4:24 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L

Peak Number 6 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.46 ug/L 611831 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS#

1 Anthracene-diO- 188 C14D10 001719-06- 2 Phenanthrene-dlO 188 C14D10 001517-22- 3 Antipyrine 188 C11H12N20 000060-80- 4 1,3,5-Triazin-2-amine, 4,6-bis(m... 188 C5H8N4S2 030358-19-1 38 Abundance Scan 3409 (23.109 min): 0503LB.D (-3404) (-) m/z 188.10 100.00% 188

5000 --------- 80 94 22.80 23.00 23.20 23.40 42 54 66 . !i p i i i । r i i i p i i i p i i i p H i p M rp-H r t ri , 132 146 158 TTTTTTTTTNTTT]*TTITNTTTTTTTT — m/z 94.05 18.65% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 188

5000 1 1 i ‘ > i ■ ■ ■ ■ । ■ i 22.80 23.00 23.20 23.40 m/Z 189.10 14.54% — 80 94 160 17 30 42 52 0 J J 108 118 132 146 | L| 170179.1,। | i P ■ । ■ P । ■ i p-i > rp i < i । I I i । p I I । p i 11 p । i i p I ■ । p i M P 11 i p < < i । ri i i p i ri p i r> ।'< i । । p > i । । rl'l'I । i ■ i TI n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ... /.......... I I I I I 1 1 I I I 1 I [ r I II I IlliP 22.80 23.00 23.20 23.40 5000 m/ z 184.05 13.51%

80 94 160 30 42 52 11I I I ' | 1 I108 66 118 132 146 I 170179,1,11 i | । । > i | i । । । | i i i । | I t > r । I I I i | I I I । । i । I I I ■ i I | I I | I I i r [ i I I I | I I I I I ( I I I I r r rI I ■. I I I | > I I i | I' II' l| I i I i | m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79725: Antipyrine T’II’1IIU*’’I 188 22.80 23.00 23.20 23.40 96 m/z 80.10 13.35%

5000 77 56 105 27 39 , 67 130 145 159 173 abas "l | 115 IL Ttr 111! i t 111 r! ’ 11 r[ 11 < 111 ri < 11111111 >< 11111111 I I I I I I I I I I I I I I I I I ■ I I I I I I 1 11111111 T I | l r i , r i i i ! | ' I I I | I I I I r /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

0503LB.D 050102.M Thu May 09 09:21:11 2002 Page 9

NYC-WTC_000045559

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NYC-WTC_000045559Source: NYC Law Department, mirrored locally

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