GCMS blank analysis results, sample AE09771, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050602\0425LB.D Vial : 16 Acq On 6 May 2002 11:56 pm Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.64 ug/L 708900 Phenanthranene - dl 0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 91 2 Phenanthrene-dlO 188 C14D10 001517-22-2 47 3 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 Pentacyclo [8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 36 Abundance Scan 3409 (23.109 min): 0425LB.D (-3401) (-) m/z 188.10 100.00% 188

5000

80 94 1 42 54 66 . J 160 22.80 23.00 23.20 23.40 132 I I I I I I I I I I I' P I f l”p I I I p. I I I I I t I I I I I I I I I I I P I I I I i1 " 11 " " i1 ‘111 +4 m/ z 94.10 15.79% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 i । । । । । > y । । -i । । । । । p । । । । । 22.80 23.00 23.20 23.40 m/z 189.10 15.18% RR 80 94 160 | fl 17 30 42 52 ° l . 108 118 132 146 | 1701791,i 4 p i i i p 11 i p i 11 p i । i p I 11 p 11 । p 11 11 —Tt |'I I । i p i । i p 111 p i i i p । I ■ । । । I > । ■ । rrp 11 । 11 i । । 11111 Wr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ----- 22.80 23.00 23.20 23.40 5000 m/ z 80.05 14.31%

80 94 160 30 , 11 42 52 66 108 118 132 146 1| 170179, I,,,.. I I I I I I I I I I I P I I I P I I I P I I I P I I I I H p ri t p l i i p i i rp i । i p ri i p i i i p i l i [ rrfT I I II [ I ! I r I I I II I I III m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79716: -(4-Tolyl)-3-methyl-pyrazol-5-one i । [ । P P । । i । । । । । । । r 188 22.80 23.00 23.20 23.40 91 m/z 184.10 9.29% 105 5000 119 65 4151... 1.. 78 TTHT 1111" i " " i " '' r " 11 L8 1’ 146 I । —|_r> rr‘ r ii । । i । । । |~rI-1" | i p V I I p i i I p i i i p i * m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

0425LB.D 050102.M Tue May 07 15:39:46 2002 Page 6

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