GCMS analysis results for unknown compounds, sample AE10201, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\05 0 8 02\10 2 01.D Vial : 19 . Acq On 9 May 2002 6:04 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method— C:\MSDCHEM\1\METHODS\050102 .M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 Anthracene-dlO- Concentration Rank 2

R.T. EstConc . Area Relative to ISTD R.T,

23.11 0.51 ug/L 790477 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Anthracene-dlO- 188 C14D10 001719-06-8 72 2 Phenanthrene-dlO . 188 C14D10 001517-22-2 72 3 4-Methyl-2-(4 - fluorophenyl)pyrim. . . 188 C11H9FN2 076128-67-1 50 4 Cycloheptanone, 4-phenyl,-188 C13H160 067688-28-2 50 Abundance Scan 3409 (23.109 min): 10201 ,D (-3402) (-) m/z 188.10 100.00% 188

5000 7 I 80 94 1 1 1 ■ ■ 1 ■ T 1 ' 1 1 1 ‘ 1 1 ' ’l 1 1 22.80 23.00 23.20 23.40 . T 43 52 66 118 132 146 158 0-TI,‘ TT , , TTTT , , THT . I l'|l I'l I | I 9 ! | ! 1 I < | > । I I | । I I । | I ! I I | I । I I | I 1 "l’ I , , I | I , ! I | I m/z 189.10 16.42% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 1 I I I 1l ' I I 'I ' I 1 1 1 1 I I 1 22.80 23.00 23.20 23.40 m/z 94.10 16.23% 80 94 160 66 17 30 42 52 J 108 118 132 146 | 170179 o111' • •' 11 " ' I''111'1111111 —HTH + T tj 1Ti | I I I I | I IT I | I I I I | I I I I ] I T I TJ't I PPp I I I I | I I I T | rl'l1 111111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120.130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ------- 22.80 23.00 23.20 23.40 5000 m/ z 80.10 15.17%

80 94 160 30 42 52 66 11 108 118 132 146 || 170179 011 I I I I I I I I I I I I I I I I I I I I I I I I J J I I I I I I I II I t I I [ I I I I | I I I I | I I I I | I I I I | I I I I | I I I 1 | I 1’"’u I I I J I ! I I | PI1!1 — m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79745: 4-Methyl-2-(4-fluorophenyl)pyrimidine I r । । — i ] i — । । । । — । । । । । i"

188 22.80 23.00 23.20 23.40 m/z 184.00 12.33% 121 5000 173 67 94 39 57 J 84 || 133 146 161 i , । । 2 । j । — । । । । । । । । । 1 । [ 0 11 pri i 11 । > > । । । । I’P। । I < r। ।'i । > i'111 11 111 i I i । । । I । r । I t 11 । r । । । ।1 TTTC0m00001BB—m0CmO—T—ur 111" I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10201.D 050102.M Thu May 09 13:37:09 2002 Page 13

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