GCMS analysis results for sample AE06407, May 3 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050102\6407.D Vial: 17 Acq On 1 May 2002 10:45 pm Operator: Mclean Sample re-ext 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 6 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.63 ug/L 624841 Phenanthranene-dlO 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 87 2 4-Methyl-2-(4 - fluorophenyl)pyrim. . . 188 C11H9FN2 076128-67-1 40 2 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 38 Abundance Scan 3409 (23.109 min): 6407. D (-3403) (-) m/z 188.15 100.00% 188

5000 / 80 94 22.80 23.00 23.20 23.40 Ami I | I ■ I I | ■ I | 41 52 66 11 132 146 158 * I I | I I I'i | I f I 1 | > 1 I I ' T I > I | I I i I | | i"i T| i I i i 1171 । I i i > । i i I i । I iJ i i i i । i । m/ z 189.15 15.40%l ‘i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

1 । । । — । । < — । । । ।—।—।—।—।—।—।—।—r 5000 22.80 23.00 23.20 23.40 m/z 94.10 15.33% 80 94 160 , । A 17 30 42 52 66 THH 11111111 r 1'111■1111111111111 108 118 132 I1"1!............. 111 " I 146.14,179179.. TT /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine 188 r । | । P । | i n । | I I I I | I I i i r

121 22.80 23.00 23.20 23.40 5000 m/z 80.20 14.82% 173 67 94 39 57 I . 84 |, । | i । i । | । । i । | < i I i | < I ( I | I IT'I"| Ti I I | । i' । । । i i i i । i I i i । I i i i MIrIl’ 133 146 161 I I > > 1 I I I ' I' I I I I I I [ > i r I I I I I I I I I i11111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 2300 23.20 23.40 m/z 184.10 13.16% 145 5000

117 41 51 63 77 89 102 1 30 ' | । । I । | ' i । ] '1 । i AI rrtltte-r rliln ] i lsp-rllr-l t r ‘p i i ] i rllp i i i i r | l'l 159 173 I 1111'" I / /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

6407.D 050102.M Thu May 02 12:26:55 2002 Page 9

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