GCMS analysis results for sample AE06407, May 3 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050102\6407.D Vial: 17 Acq On 1 May 2002 10:45 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Phenanthrene, 9-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.30 ug/L 297850 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C.11H12O3 004497-40-9 42 3 1H-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5/ 2 4 2-Imidazolidinone, 1-methoxy-3-p.. . 192 C10H12N2O2 052420-43- 38 Abundance Scan 3319 (22.580 min): 6407.D (-3312) (-) m/z 192.10 100. 00% 192

5000

_ 92 96 146 ..... ..... A 22.20 22.40 22.60 22.80 23.00 4P 52 70 । .1 118 | 160 I | r । I I | । r 1 I | I I । । | I > । ' | I I I I [ । । i । | I I I I ] I I I । | । । ! I | I I > । | । । < > | I I F I | > » I > | > I I ( | I । m/z 191.10 17.71% 11111 ■ ।‘ T-p-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 ................... 1 1 1 1 1 1 I 1 1 1 1 I 1 1 1 I I 1 ' 1 • I ' 22.20 22.40 22.60 22.80 23.00 m/ z 193.10 14.92% 96

m/z-> 29 39 51 63 74 83 / 115 126 139 152 I | r i r i | i i | | | | 1 i i | i i i i | I' i i | | i I' I i | I i r I | I I 1 > | i । | t | | t t r ym f i । । । । ।' । i i i > | ’ I । । । ।

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 165 lTTTTH 176 l— Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161 1 I ' 1 1 1 i 1 1 1 1 I ' 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 14.34% 77 121 149 177 9 103 m/z-> 52 64 ! p > I ■ p > I l p I > > p [> > > p ' । I ! p > < । p I I I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 + .172.1.. ...... ....I Abundance #80945: 1 H-2-lndenone,2,4,5,6,7,7a-hexahydro-3-(1-methylet... 192 22.20 22.40 22.60 22.80 23.00 -4 149 m/z 96.00 11.96% 177 A 5000 41 164 55 67 79 93 107 121 135

m/z-> T-p-r 27 4+ +4+4+4l 4474+ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 T HHT ' 11' 1 ... (I.. II. 22.20 22.40 22.60 22.80 23.00

6407.D 050102.M Thu May 02 12:26:55 2002 Page 8

NYC-WTC_000044552