GCMS sample analysis results, AE11906, June 3, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11906.

NYC-WTC_000012966–000012988

Folder label: “GCMS X 5-21-02 A 5-22-02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11906.D Vial: 13 Acq On : 22 May 2002 11:36 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 13 Phenanthrene, 9-methyl- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.28 ug/L 326512 Phenanthranene-dl0 22.92 Hit# of 5

1 Phenanthrene, 9-methyl- Tentative ID MW 192 C15H12 MolForm CAS# 000883-20-5 53PP oualQ 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 3 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 37 ( 4 Anthracene, 1-methyl- 192 C15H12 000610-48-0 36 — Abundance Scan 3312 (22:539 min): 11906.D (-3304) (-) m/z 192.10 100.00% 19/2

5000

42 54 66 R2 । 96 I 146 160 22.20 22.40 2260 22.80 1 A /z-> 0 11 > 1111111-]411 r| 11111,1111 i > i 1111 i 111 H 111 >' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 C 4 m/z 191.10 19.41% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 ■ ■ i * > ■ ■ । ' > ■ ■ । *1 i 1 1' 1 i 22.20 22.40 22.60 22.80 m/z 146.10 16.87% 96 ice 29 39 51 63 74 83 115 126 139 152 0176 J, [ 0 ' l " ‘ ‘ I “ ‘ ‘ I ‘ " ■ I ‘ ‘ mn | > "r rh rh 'll1 r 11 11 ",| Ipummyeg 1 n ]•! 1111 i'lS ’1 I fl-1111 ‘ 111 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161 --------------------- 22.20 22.40 22.60 22.80 5000 m/z 96.10 15.33% 77 14991 177 103 121 52 64 t138

m/z-> 0------ Ml Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80907:2-lmidazolidinone, 1-methoxy-3-phenyl- 192 .. 0. ). 106 22.20 22.40 22.60 22.80 m/z 193.00 14.20% 77 119 162 5000 42 56 91 4 w++ + 111 m-| . 1. ''I | ‘ I „ 1111111111 111111 L > > | > > > < । < ■ ■ i j Ln । > i 0 • * i > • * • i * < miz—> 20 30 40 50 60 70 80 90 100110120 130140 150 160170 180 190 200 22.20 22.40 22.60 22.80

11906.D 052202.M Tue May 28 12:13:27 2002 Page 16

NYC-WTC_000012986

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GCMS sample analysis results, AE11907, June 4, 2002 · Box DEP Box 15

NYC-WTC_000012989

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.

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