GCMS blank analysis results, sample AE12288, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report

t Data File : C:\MSDCHEM\l\DATA\052902\LB.D Vial: 4 Acq On : 29 May 2002 12:32 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 14 Phenanthrene, 9-methyl- Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.22 ug/L 197656 Phenant hranene- dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 3 lH-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5 42 4 2-Imidazolidinone, 1-methoxy-3-p. . . 192 C10H12N202 052420-43-6 38 Abundance Scan 3311 (22.533 min): LB.D (-3305) (-) m/z 192.00 100.00%| 192

5000

146 - 40 49 66 82 %6 160 22.20 22.40 22.60 22.80

mfz~> Ol- TT-T kpmmm m/z 146.00 18.97%| 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 .................. A1 ............. ■ ■ i ' ‘ 1 1 i ‘ i ■ ■ ■ ■ I 1 22.20 22.40 22.60 22.80 L * • • I

m/z 191.00 17.50%l 29 39 51 63 74 83 * 115 126 139 152 165 176 । 0- ' 1 “ ' ‘ I “ "I' ‘ " I “ " Ifl “ I'11 ’ f11 r ‘1'11" 111'1'1'111111 > । > 11 i’i ।।' |‘i 111 ye’rt 111 rht 111 rTt ■ * i ‘ ‘ miz-> 2030405060 70 8090 100 110 120 130 140 150160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxypheny!)- 192 161 22.20 22,40 22.60 22.80 5000- m/z 193.10 14.05% 77 91 121 149 177

miz-> 0 52 . ................ 1 ..... I 64 i ■ ■ ■ ■ i1 , l. 103

20 30 40 50 60 70 80 90 1OO 110 120 130 140 150 160 170 180 190 200 138 + Abundance #80945:1 H-2-lndenone,2,4,5,6,7,7a-hexahydro-3-(1-methylet... * • i > * ■ ■ i > • i ‘ ' 1 i ■ 3I 192 22.20 22.40 22.60 22.80 149 m/z 96.10 12.10% 177 5000 41 93 164 27 55 67 79 107 121 135 , - ■ ■ I .1 kll +4++ fUrrj 11 A I, M hrya hotor nirp + . . I. A O' ’I /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

LB.D 052202.M Mon Jun 03 09:27:24 2002 Page 17

NYC-WTC_000014174