GCMS blank analysis results, sample AE12288, June 2002

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Data File : C:\MSDCHEM\1\DATA\052902\LB.D Vial: 4 $ Acq'On : 29 May 2002 12:32 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 Anthracene-dlO- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.27 ug/L 241909 Phe nant hranerie-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 86 2 Phenanthrene-dlO 188 C14D10 001517-22-2 78 3 Antipyrine 188 C11H12N2O 000060-80-0 50 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3401 (23.062 min): LB.D (-3394) (-) m/z 188.10 100.00% 188

5000

80 94 158 40 22.80 23.00 23.20 23.40 0- " I “ 1 H < । ‘ ■ 11 i' 111 i n 1111 r| > ri 11 r mTPHFri '' | ‘ । m/z 94.10 18.15% mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 184.10 18.02% ce 80 94 160 17 30 0 'I'" > C 11T'1 -42..52.98++++=+,108118.132. 146+179179 TTnm mfa-> 10 20 30 40 50 60 70 80 90 100110120130140150 160170180190 Abundance #79827: Phenanthrene-d10 188 ........... ,................................. 22.80 23.00 23.20 23.40 5000 m/z 80.00 14.52%

80 94 160 30 42 52 66 , 1[ 108118 132 146 11, 170179,1,11 0 11111 rj'i 111 111 j 111111 [ l‘H 111 H 11 r i 1TF | It II | I I <1 | 1 1 | I [i 111] 1 I 1'1 | 1 rl’l’ rTTp m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79725: Antipyrine 188 — ) 14 — 1 i • ■ • ' i ■ • 22.80 23.00 23.20 23.40 96 m/z 189.10 13.28% 5000 77 56 105 39 0- ............................... m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

LB.D 052202.M - Mon Jun 03 09:27:24 2002 Page 18

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