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GCMS analysis results for sample AE10163, May 2002

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Laboratory report showing GC/MS analysis results for sample AE10163 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023472–000023486

Folder label: “GCMS X 5/9/02 A 5/13/02

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NYC 9/11 Public Portal Document * Data File : C:\MSDCHEM\l\DATA\051302\10163.D Vial: 11 Acq On : 13 May 2002 7:38 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 23.11 0.39 ug/L 458838 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 87/ 2 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 38 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 38 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 Abundance Scan 3409 (23.109 min): 10163.D (-3403) (-) m/z 188.10 100.00%! US

5000

94 80 22.80 23.00 23.20 23.40 42 54 66 118 132 160 ,...... 0 TIPTTTTTTTPPTTT TmTTTTTTTTT 1 ■ 'i" "T m/z 94.10 17.88%| /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- US

5000 ............ .. 22.80 23.00 23.20 23.40 m/z 189.15 15.27%| 17 30 42 52 AK 66 80 , 94 J 108 118 132 160 ,I 146 I 170179 ,i 0 1)WWUm—umt SGaySdndpaBasnuanq —munyre l-.p'I'I'l'nM ,.,.,11'1'11 211li mfa-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79801: 2,2,9,9-Tetramethyldec-5-ene-3,7-diyne US 173 ..................................................... 41 131 143 22.80 23.00 23.20 23.40 91 5000 77 158 m/z 184.10 12.96%| 57 119 27 67 105

m/z-> 0 M l p-TTt f l l 4 + i 44l illszytlirpropaa/ 11 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 — T I FTTTT

Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/z92.10 11.92%| A 145 5000

117 41 51 63 77 89 102 1 130 159 173 mfe-> 0 । TTY । ■ i 11 j ■ n-i ‘I- i rllrr rllr । i ilr i l l'J|M i i i'I'I i 11 i rll i i i l'|-l-i i 11 rI । i 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 II ........ / ’ 1 I • • l T ' I ■ 22.80 23.00 23.20 23.40 1 1 1 1 1 1 1

10163.D 050102.M Tue May 14 11:41:28 2002 Page 8

NYC-WTC_000023484

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NYC-WTC_000023484Source: NYC Law Department, mirrored locally

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