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GC/MS analysis results for sample AE11413, May 28 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11413 conducted on May 28, 2002.

NYC-WTC_000025274–000025288

Folder label: “GCMS X 5/15/02 A 5/18/02

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Scanned page image, NYC-WTC_000025286
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NYC 9/11 Public Portal Document Y wpuiL IC POL L

Data File : C:\MSDCHEM\1\DATA\051702\11412.D Vial: 21 Acq On : 18 May 2002 5:54 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Anthracene-diO - Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.36 ug/L 421142 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 47 ' 2 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 4H-Pyrido[1,2-a]pyrimidin-4-one,. 188 C11H12N2O 057773-19-0 38 Abundance Scan 3409 (23.109 min): 11412.D (-3403) (-) m/z 188.15 100.00% 188

5000

94 158 22.80 23.00 23.20 23.40 0- i11111 40 ' i' । "'i52 111111 66 ~~ i'1180, U " " 11 ' r 132 ■ r " ' i11111" 1111" ' i' m/z 94.05 20.77% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 rn/z 189.10 15.11% 80 94 160 , . 17 30 42 52 66 J , 108 118 132 146......... 0 TTTTTTTTTTTTTTTTTHTTTTTT mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 11.46% 143 89 115 51 64 76 | 102 I, 130 i 158 170 l- 0 11............ .......... ui/" I1!1! [ I I lT| I I I 1 | I I'l I | I PPl |

m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline * 1t8 22.80 23.00 23.20 23.40 m/z 158.05 10.73% 145 5000

117 159 173 m/z-> 41 51 130 63 77 0 --------++-++++---+4---------+---#---+ - 89 102

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I 22.80 23.00 23.20 23.40

11412.D 050102.M Tue May 21 15:55:49 2002 Page 8

NYC-WTC_000025286

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