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GCMS analysis results for sample AE10810, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10810 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046006–000046035

Folder label: “GCMS X 5/7/02 A 5/15/02

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NYC 9/11 Public Portal Document

’ Data File : C:\MSDCHEM\1\DATA\051402\10810.D Vial: 20 Acq On : 15 May 2002 5:50 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene-d10- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.38 ug/L 485952 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 94 2 Phenanthrene-diO 188 C14D10 001517-22-2 47 3 4-Methyl-2-(3-fluorophenyl)pyrim. . . 188 C11H9FN2 076128-66-0 42 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3409 (23.109 min): 10810.D (-3403) (-) m/z 188.10 100.00% 188

5000

I I I I I I I TI I I + I ~l' I ‘ l l l ,

160 94 43 57 66 80 , 22.80 23.00 23.20 23.40 0 mmmmmmmmmto I i | i i । i | r i < i । 1 136 i / i । i i r i | i । i.il. I'f | > I i i j i m/ z 94.05 14.14% i'" ■ i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

/ 5000 T“1 । i i i i । i i I i | I I I I | I I ! I ]

22.80 23.00 23.20 23.40 m/z 184.10 13.52% — 80 94 160 66 । । 17 30 42 52 0 11 । r i i i | i i r i । i i i r | I i i i । I I l । Trt Ip । 4+ 108 118 132 146 I I I I I I I I I I I I I I I I I I I I I I I I । 179179, TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 189.05 10.59%

80 94 160 30 42 52 66, 108 118 132 146 1 170179 miz-> 0 / । i । i । । । i r । Ti r 11 11 ri t[ rl i < । 11 I > । (i 11 TTTTT rr|l r-ri । I i | । I I I | I I । i | I r I r ITtMTrs 1IIII |^tH4l 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 P Abundance #79744:4-Methyl-2-(3-fluorophenyl)pyrimidine *II*//*‘1IIIIIII**‘i 188 22.80 23.00 23.20 23.40 m/z 160.05 9.30%

5000 121

67 173 94 39 50 | , 82 1, 108 | 134 146 161 | - 0 —PPWTTTTTTt Tppu > ! I > ! I | I TTTTPTTTTTTTTT 1 11 '"I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10810.D 050102.M Thu May 16 12:39:34 2002 Page 11

NYC-WTC_000046021

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NYC-WTC_000046021Source: NYC Law Department, mirrored locally

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