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GCMS analysis results for sample AE10809, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10809 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045984–000046005

Folder label: “GCMS X 5/7/02 A 5/15/02

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Scanned page image, NYC-WTC_000046003
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\DATA\051402\10809.D Vial : 19 Acq On : 15 May 2002 5:01 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.45 ug/L 759524 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 93 2 Phenanthrene-dlO 188 C14D10 001517-22-2 50 3 Cycloheptanone , 4-phenyl- 188 C13H160 067688-28-2 50 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3409 (23.109 min): 10809.D (-3402) (-) m/z 188.10 100.00% 108

5000

1 ' 1 1 1 1 1 T ' ' 80 94 22.80 23.00 23.20 23.40 118 132 146 160 L m/z-> 0 43 57 66 ' I | I i | I j i ( i | | rI I 1 i i | i I | S [ i I I i |'i i I l'|

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 i r | Fl ~i l j r i i i [ H i r [ r rf Ti t T I '|'l । 1 I | । I । f | । ri1 U m/z 189.15 14.37%

Abundance #79826: Anthracene-d10- 188

/ 5000 ’ 1 ’ 1 1 ’ 11+1’1 22.80 23.00 23.20 23.40 m/ z 94.10 13.26% 80 94 17 30 42 52 66 0 111 ‘'111 । i r । i i i i ] t i i i । I I i r rt ---H 108 118 132 i r| 1 1 i 1 ] ri i i [ ri i i ] I i t 146,1170179 l— TT /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ... /........... 1 ■ । ■ ■ 1 11 ■ ' 1 1 । ' 1 1 1 । 1 ■ ■ 1 । 22.80 23.00 23.20 23.40 5000 m/z 184.10 12.40%

80 94 160 30 42 52 68 , 11I I t i | ! I108 118 132 146 ,|,[ 170179,|,|| 0 11 । < । । i । < i । i । । i । I | I i i i । I I i i । । I I i । i i r I I । । I 1 I I । I 1 I I i II [•! I I I [I I I'l I I iM'Ppi I I i | ri I r| Htt ri i i

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- / 188 22.80 23.00 23.20 23.40 117 m/z 80.10 11.01% 104 91 160 5000 131 170 27 39 51 65 78 145

m/z-> o । । >■ । । । । > > । । । । > , , । ,lt | lp ml Pi nr 7 ""i" 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 L - 22.80 23.00 23.20 23.40

10809.D 050102.M Thu May 16 12:37:47 2002 Page 15

NYC-WTC_000046003

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NYC-WTC_000046003Source: NYC Law Department, mirrored locally

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