NYC 9/11 Public Portal Document
OCaL’ii totpOulU RCDOL L
Data File : C:\MSDCHEM\1\DATA\051702\11412.D Vial: 21
Acq On : 18 May 2002 5:54 am Operator: Mclean
Sample : 5/15 eh Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 6 4-Amino-3-[p-chlorophenyl]-... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
34.90 0.23 ug/L 142823 Perylene-d12 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Amino-3-[p-chlorophenyl]-1-met... 259 C12H10C1N5 1000214-63-7/9
2 2-Methyl-6-phthalimido-hexan- 3-one 259 C15H17NO3 1000213-32-0 9
3 4-Piperidinemethanol, 1-methyl- 129 C7H15NO 020691-89-/ 9
4 Naphthalene, 1,2,3,4-tetrahydro-... 177 C1OH11N02 029809-14/1 9
Abundance Scan 5416 (34.901 min): 11412.D (-5415) (-) m/z 44.05 100.00%
44 130
259
86 118 207
5000
34.60 34.80 35.00 35.20
0—T ' 1 i ' ■ ■ 1 i ■ ■ ■ 1 i 1 m/z 129.70 92.02%
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260
Abundance #94490: 4-Amino-3-[p-chlorophenyl]-1 -methylpyrazolo[3,4-d]...
259
)....................................
5000
34.60 34.80 35.00 35.20
43 m/z 259.00 62.39%
75
mlz->
0
86
llyil++
40
22,111 126 138149/s1176 189,204216.731,243,.
60 80 100 120 140 160 180 200 220 240 260
Abundance #4597: 2-Methyl-6-phthalimido-hexan-3-one
4
160 216
34.60 34.80 35.00 35.20
5000 174 m/z 127.30 56.13%
77
130 188 259
104
148
o1 TTH 11 90 .11117
TU"rfdi "r I ..I —
201 I.......... 244
TI ‘IIIIIITTTI
o.....
T" 1 1 i ■ 1
m/z-> 40 60 80 100 1 20 140 160
180 200 220 240 260
Abundance #10568: 4-Piperidinemethanol, 1 -methyl-
1 1 1 1 1
44 34.60 34.80 35.00 35.20
m/z 128.00 53.28%
5000 128
55
70 98
112
|IL|
0 1 1T1 1 ' | 1 1 H | ।
—
I"11 ‘
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20
11412.D 050102.M Tue May 21 15:55:51 2002 Page 9
NYC-WTC_000025287
OCR can misread numbers and units. Confirm readings against the page image before using them.