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GC/MS analysis results for sample AE11413, May 28 2002

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Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11413 conducted on May 28, 2002.

NYC-WTC_000025274–000025288

Folder label: “GCMS X 5/15/02 A 5/18/02

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NYC 9/11 Public Portal Document OCaL’ii totpOulU RCDOL L

Data File : C:\MSDCHEM\1\DATA\051702\11412.D Vial: 21 Acq On : 18 May 2002 5:54 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 4-Amino-3-[p-chlorophenyl]-... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 34.90 0.23 ug/L 142823 Perylene-d12 34.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Amino-3-[p-chlorophenyl]-1-met... 259 C12H10C1N5 1000214-63-7/9 2 2-Methyl-6-phthalimido-hexan- 3-one 259 C15H17NO3 1000213-32-0 9 3 4-Piperidinemethanol, 1-methyl- 129 C7H15NO 020691-89-/ 9 4 Naphthalene, 1,2,3,4-tetrahydro-... 177 C1OH11N02 029809-14/1 9 Abundance Scan 5416 (34.901 min): 11412.D (-5415) (-) m/z 44.05 100.00% 44 130

259 86 118 207 5000

34.60 34.80 35.00 35.20 0—T ' 1 i ' ■ ■ 1 i ■ ■ ■ 1 i 1 m/z 129.70 92.02% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #94490: 4-Amino-3-[p-chlorophenyl]-1 -methylpyrazolo[3,4-d]... 259 )....................................

5000 34.60 34.80 35.00 35.20 43 m/z 259.00 62.39% 75

mlz-> 0 86 llyil++ 40 22,111 126 138149/s1176 189,204216.731,243,. 60 80 100 120 140 160 180 200 220 240 260 Abundance #4597: 2-Methyl-6-phthalimido-hexan-3-one 4 160 216 34.60 34.80 35.00 35.20 5000 174 m/z 127.30 56.13% 77 130 188 259 104 148

o1 TTH 11 90 .11117 TU"rfdi "r I ..I — 201 I.......... 244 TI ‘IIIIIITTTI

o..... T" 1 1 i ■ 1 m/z-> 40 60 80 100 1 20 140 160 180 200 220 240 260 Abundance #10568: 4-Piperidinemethanol, 1 -methyl- 1 1 1 1 1 44 34.60 34.80 35.00 35.20 m/z 128.00 53.28% 5000 128 55 70 98 112 |IL| 0 1 1T1 1 ' | 1 1 H | । — I"11 ‘ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20

11412.D 050102.M Tue May 21 15:55:51 2002 Page 9

NYC-WTC_000025287

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NYC-WTC_000025287Source: NYC Law Department, mirrored locally

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