GCMS analysis results for sample AE10134, May 8 2002

NYC 9/11 Public Portal Document

'Data File C:\MSDCHEM\1\DATA\050202\10134.D Vial: 26 Acq On 3 May 2002 9:42 am Operator: Mclean Sample 4/29 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Chroman[2,3-e]pyrimidine-2 -... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

34.94 0.22 ug/L 104751 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# -al

1 Chroman[2,3-e]pyrimidine-2-one, ... 262 C13H14N2O4 1000116-59-9 9 2 Imidazole, l-methyl-2-methylthio- 128 C5H8N2S 1000126-41-3 9 3 1,3-Dimethyl-3,4,5,6-tetrahydro-... 128 C6H12N20 007226-23-5 9 4 2-Propenal, 3-(dimethylamino) -2-... 128 C6H12N20 0495/2-62-9 7 Abundance Scan 5422 (34.937 min): 10134.D (-5420) (-) m/z PVMy—MMMMM 40.0 100.00% 43

262 128 5000 281 207 111111 1 1 11 11 1‘*I‘‘‘‘I 34.60 34.80 35.00 35.20 ■ i ■ ' 184 m/z 262.20 71.17% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #94914: Chroman[2,3-e]pyrimidine-2-one, 1,2,3,6-tetrahydro... 262

5000 247 34.60 34.80 35.00 35.20 . 133 m/ z 128.00 54.59% 49 64 77 96 148, 176 191204 TUt -11281401—41 ■ 160.1,1.218230 ... ... ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #58013: Imidazole, 1 -methyl-2-methylthio- 128 95 72 34.60 34.80 35.00 35.20 42 m/z 129.50 45.15% 5000 fl 113 54

"dt 44 40 60 +4— li........... 11 1 1 1 1 1 1 I 1 1 1 1 I 80 100 120 140 160 180 200 220 240 260 280 /z-> 20 Abundance #57896:1,3-Dimethyl-3,4,5,6-tetrahydro-2(1 H)-pyrimidinone T‘ ] । । i r II 1 I | i i i i । i r-1 I i" 128 34.60 34.80 35.00 35.20 42 m/z 281.10 42.35%

5000 28 57 70 99 II 84

n/z-> . . Jil— " i 1 1 20 40 ------ 113

80 100 120 140 160 180 200 220 240 260 280 lil 34.60 34.80 35.00 35.20

10134.D 050102.M Mon May 06 12:24:24 2002 Page 17

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