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GCMS analysis results for sample AE10810, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10810 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046006–000046035

Folder label: “GCMS X 5/7/02 A 5/15/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\051402\10810.D Vial: 20 Acq On : 15 May 2002 5:50 am Operator: Mclean Sample : 5/7 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L **************************************************************** * * * * * Peak Number 13 lH-Indene, 2,3-dihydro-1-me... Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

35.06 0.24 ug/L 211013 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1H-Indene, 2,3-dihydro-l-methyl -... 208 C16H16 006416-39-3 9 2 Thiophene, 3-(methylthio) - 130 C5H6S2 020731-74-2 9 3 Propane, 2,3-dichloro-l,1,1-trif... 166 C3H3C12F3 000338-75-0 9 4 5-lodohistidine 281 C6H8IN3O2 1000131-15-8 9 Abundance Scan 5444 (35.066 min): 10810.D (-5441) (-) m/z 129.90 100.00% 130 208

56 259 _ 5000 81 115 281 43 I I 1 f 1 I I I I I I I > I I I I I I

34.80 35.00 35.20 35.40 01 ■ r i ■ 1 ‘ ■ I I.... .86.... TTT I 1 1 1 1 1 m/z 2 08.10 89.68% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #85090: 1H-lndene, 2,3-dihydro-1-methyl-3-phenyl- 208 193

5000 115 130 178 34.80 35.00 35.20 35.40 91 m/Z 56.00 55.46% 165 Of 27, 51477 mi 4, I i i | i iii । I r l " । I i i TIu r r | r i il | i i 152 +r I ' ' 1 ' I m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #58658: Thiophene, 3-(methylthio)- 130 AMAAMAAl 34.80 35.00 35.20 35.40 5000 45 115 m/z 259.10 55.16% 71 84 97

29 I 58 । 01 144 TIIil, mm "'h 1 1 i ' I Lil

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #58659: Propane, 2,3-dichloro-1,1,1-trifluoro- 130 ■ 34.80 35.00 35.20 35.40 49 m/z 260.20 52.21% 98 5000 69 85 166 27 111 0 14 1 1 1 . 1 r1 1 . — 1, 4 ll, r ।. 1 147 ..................................... 11 i 1 1 Il I I 1 II I lr > I I I I , I I Illi il I I 1; I I I I I I rOOIs I । । ।r I । । । । । । । i |'”r i । i' । i r

m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.80 35.00 35.20 35.40

10810.D 050102.M Thu May 16 12:39:49 2002 Page 17

NYC-WTC_000046027

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NYC-WTC_000046027Source: NYC Law Department, mirrored locally

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