GCMS analysis results for sample AE09335, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9335.D Vial: 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Silane, (4-bromophenoxy)tri.. . Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 37.21 0.26 ug/L 305663 Perylene-dl2 34.73

Hit# Of 5 Tentative ID MW MolForm CAS# Qua

1 Silane, (4-bromophenoxy)trimethyl- 244 C9H13BrOSi 017878-44-3 /9 2 2H-Phenanthro[9,10-b]pyran 232 C17H120 000217-67-4 7 3 lH-Thioxanthene-4-carboxaldehyde... 232 C14H160S 019809-87-1 7 4 3-Buten-2-ol, 4-(2,2,6-trimethyl. . . 210 C13H2202 051138-08-0 7 Abundance Scan 5810 (37.216 min): 9335.D (-5801) (-) m/z 119.00 100.00% 40 711 95 1 9 149 231 135 165 215 | 57 5000 1C7 191 281 __ii j i । i i [ । r i r i r i t i r r 1—ll—i 83

m/z-> 20 40 L ' ' i 1 60 J 80 TTT i-r F'T-r i । । m , ! i । i । । । '> । । i‘| i 1 [ i 100 120 140 160 180 200 220 I ] i i m [1 i i i p r 240 260 280 36.80 37.00 37.20 37.40 37.60 m/ z 40.10 99.08% Abundance #89846: Silane, (4-bromophenoxy)trimethyl- 231 139 244 5000 1 1 i 1 1 115 36.80 37.00 37.20 37.40 37.60 91 m/z 71.10 99.08% 155 M 201 । > j 1 i i । । i | । । i r 0 " ' i"1" l"' 1 I ll

hmhuaduuLA 1 1 । 1 ■ ' 1 i' 1 1 1 ■ । ' /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #90049: 2H-Phenanthro[9,10-b]pyran 2 12

36.80 37.00 37.20 37.40 37.60 202 m/z 149.00 94.95% 5000

/z-> Abundance 116 },7,1‘‘1‘111I‘/II rrrl i 1 ' -1 I I I 17 I I I I I i ! I I I I I- 20 40 60 80 100 120 140 160 180 200 220 240 260 176

#90012:1H-Thioxanthene-4-carboxaldehyde, 2,3,5,6,7,8-hexa... —H

203 i 215

232 280 hrus 36.80 37.00 37.20 37.40 37.60 m/z 231.20 93.12% 29 5000 215 45 115 n 91 128141 161 175 189 65 — —4441444alll—B I ll ' ... “WAPMwAM A______ — ———— 1 i 1 ’ ' ■ i ' ■ 1 1 i ' 1 | । 1 1 । | 1 । i i । r rn |—11—i—i—।—i—r m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 36.80 37.00 37.20 37.40 37.60

9335.D 050102.M Mon May 06 13:59:59 2002 Page 21

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