GCMS analysis results for sample AE10810, May 2002

NYC 9/11 Public Portal Document

' Data File : C:\MSDCHEM\1\DATA\051402\10810.D Vial: 20 Acq On : 15 May 2002 5:50 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 20 9,12,15-Octadecatrienoic ac... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

37.77 0.62 ug/L 551891 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 9,12,15-Octadecatrienoic acid, 2... 496 C27H5204Si2 055521-22-7 10 2 2-(2,6,6-Trimethylcyclohex-1-eny. .. 222 C14H2202 1000185-64-1 9 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 9 4 1-Monolinoleoylglycerol trimethy... 498 C27H54O4Si2 054284-45-6 9 Abundance Scan 5904 (37.769 min): 10810.D (-5887) (-) m/z __ 73.10 100.00% 73 147 221 5000 295 356 429

a 41 103 267 1 ' 1 1 1 i 1 191 37 40 37.60 37.80 38.00 38.20 01 - m/z 147.00 78.77% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #25608: 9,12,15-Octadecatrienoic acid, 2,3-bis[(trimethyls. . 29 73 147 220 5000 109 37 40 37.60 37.80 38.00 38.20 191 281 m/z 221.05 66.13% 0 LZALLAmti 192, LALLL333 rf 355377 T 1 . 1 249 303 409 435 483 ’tm i L1 i ■ i r ■ i n/z-> 50 100 150 200 250 300 350 400 450 Abundance #66034: 2-(2,6,6-Trimethylcyclohex-1 -enyl)cyclopropanecarb... 147 I | I | । | । । । 11H 11 । । | r I I I | I 37.40 37.60 37.80 38.00 38.20 107 m/z 207.00 45.71% 5000 175 207 41 79 wyAAPA/MhaM-wwM m/z-> 0- ulad. A 1—4 50 100 150 200 ' 250 i 1 1 ■ 1 300 i ■ 1 ■ ' 350 i ' 1 ■ ■ 400 i 1 1 1 1 450 i 1 1tl Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... TIT I 1 1 1 1 i ' 73 37.40 37.60 37.80 38.00 38.20 147 m/z 295.00 41.98%

5000 281 45 369

m/z-> 0- TlrL 50 117 1 i ' '' 100 t

150 " i I I 207 2/19 , I | 4 r -1 200 1 250 1 i 300 350 400 450 Tl v T' 1 1 ' 1 1 ' 6lI ‘ ‘‘4" 37.40 37.60 37.80 38.00 38.20

10810.D 050102.M Thu May 16 12:40:09 2002 Page 24

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