Laboratory report of a GCMS blank run conducted on May 14, 2002, showing non-detect results for various compounds.
NYC-WTC_000022965–000022989Folder label: “GCMS X 5/8/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\MSDCHEM\1\DATA\050902\0508LB.D Vial: 4 Acq On 9 May 2002 5:43 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 Cyclononasiloxane, octadeca... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 39.34 0.99 ug/L 637888 Perylene-dl2 34.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclononasiloxane, octadecamethyl- 666 C18H54O9Si9 000556-71-8 59 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 25 3 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 23 4 2,6-Dimethyl-3,4-bis(trimethylsi ... 311 C15H29NO2Si2 1000079-52-1 12 Abundance Scan 6172 (39.343 min): 0508LB.D (-6156) (-) m/z 147.10 100.00% 73 147 221
5000 355 281 . A4-A I 429 40 503 39.00 39.20 39.40 39.60 0- apopogum . .......... — - _______ 1____________________ ' I ' 1 ' ' I 1 ' ' 111 I I I I I I I I [ I I m/ z 73.10 99.48% n/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429
355 5000 281 39.00 39.20 39.40 39.60 m/z 221.00 76.34% 475
n/z-> 0- 0 —4 i ■ ■ ' ■ i ' • ' ■ i ■ ■ 50 100 150 200 250 300 350 400 IIi 450 500 550 600 650 651
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)... 73 147 39.00 39.20 39.40 39.60 5000 267 m/z 355.00 48.81%| 355 429 207
_ 0 I . ........ 1471 1 ’ ’1 ’ I ... I ’+1’ +*4I141 ................. _ +*+I1+-1+1’’ I’’ ■ l ■ • ■ - । ‘ । i TT’ । । । । । । । । । । niz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)- 1 ' I 1 1 1 ' 1 1 73 39.00 39.20 39.40 39.60 147 m/z 207.00 41.21% 5000
221 nw/lutulnopo m/z-> 0 +13.14. '■ 1/ r 147— 0 50 104 100 150 200 250 300 350 400 450 500 550 600 650 ' 1 i 1 ■ ‘ 1 1 ' ' ■ ' 1 1 ' 1 ' i ' 39.00 39.20 39.40 39.60
0508LB.D 050102.M Tue May 14 10:15:02 2002 Page 20
NYC-WTC_000022988
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NYC-WTC_000024041
Laboratory report showing non-detectable levels of nitrosamines and other contaminants in blank sample AE10895.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025216
Laboratory report showing GCMS blank analysis for sample AE11410 conducted on May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023409
Laboratory report showing non-detect results for volatile organic compounds in a method blank sample AE10137 analyzed on May 14, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023925
Laboratory report showing GC/MS analysis of sample AE10982 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023991
Laboratory report showing GC/MS analysis of sample AE10984 with surrogate recovery data for 2,4-DDD.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025102
Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023949
Laboratory report showing GC/MS analysis of sample AE10983 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045936
Gas chromatography-mass spectrometry blank analysis conducted May 17, 2002 testing for semivolatile organic compounds with all results below method reporting limits.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044559
Laboratory report showing blank test results for various organic compounds on May 7, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013883
Fragmented document header from DEP Box 15 archive containing metadata for environmental testing records dated late May 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046006
Gas chromatography-mass spectrometry report for sample AE10810 showing detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044381
Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for organic compounds.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000022961
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000022962
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder
NYC-WTC_000022990
Laboratory report documenting GCMS calibration verification analysis conducted on May 14, 2002.
Filed in the same folder
NYC-WTC_000022994
Laboratory report of GCMS reference standard analysis conducted on May 14, 2002, showing recovery percentages.
Filed in the same folder
NYC-WTC_000023002
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder