NYC 9/11 Public Portal Document
aLy DcaLtii OpOUlIU RCDOL L
Data File : C:\MSDCHEM\1\DATA\051702\11380.D Vial: 7
Acq On : 17 May 2002 5:40 pm Operator: Mclean
Sample : 5/15 ad Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 10 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
35.41 0.50 ug/L 358077 Perylene-d12 34.70
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 33
2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 27
3 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25- 23
4 Trisiloxane, 1,1,1,5,5,5-hexamet .. 384 C12H3604Si5 003555-47-3 16
Abundance Scan 5503 (35.413 min): 11380. D (-5491) (-) m/z 73.10 100.00%
73 147 221
281
5000 355
munoroow) yoobwiy
96 429
191 35.00 35.20 35.40 35.60 35.80
m/z->
0-
44
II-
50
LL
' i '
100
T
150
i r—i
200
i—|—>
250
I,
300 350
I I, — 1.
400
m/Z 147.10 98.11%
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)...
73
147
5000 267
355 429 35.00 35.20 35.40 35.60 35.80
45 207
m/z 221.10 84.23%|
m/z->
o1 I
50 100 150 200
|............. I I
250 300 350
-l
400
Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime...
73 147
■ 1 ' । 1 ■
281 35.00 35.20 35.40 35.60 35.80
5000 m/z 280.95 50.20%|
45 369
1 , 95 117 177 297226 249 ! 310 341 .
m/z->
0-
50
1/ 7 "1
100
— ' " * hen
150 200
r 1*
250 300 350 400 ulw/ WAnhayMa
Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7...
147 221 35.00 35.20 35.40 35.60 35.80
m/z 355.00 42.81%|
73
5000
191
117 279
45 ih1 1 L ' 1 1,‘ 249 I ............
0 T- 11II ■ i r 1 ’ ■ i 1 1 1 ' i 1 1 1 ' i 1 T1 1 1 1 I '
n/z-> 50 100 150 200 250 300 350 400 35.00 35.20 35.40 35.60 35.80
11380.D 050102.M Mon May 20 15:46:53 2002 Page 13
NYC-WTC_000025122
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