NYC 9/11 Public Portal Document
Llbrary searen compound Report
Data File : C:\MSDCHEM\1\DATA\051702\11380.D Vial: 7
Acq On : 17 May 2002 5:40 pm Operator: Mclean
Sample : 5/15 ad Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C : \DATABASE\NI ST 9 8 . L
*********************************************************************
Peak Number 11 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
36.49 0.68 ug/L 486939 Perylene-dl2 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0/27
2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47 22
3 2,6-Dimethyl-3,4-bis(trimethylsi... 311 C15H29NO2Si2 1000079-52-1 12
4 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-/3-9 12
Abundance Scan 5687 (36.494 min): 11380.D (-5677) (-) m/ z 73.05 100.00%
73 147 221
5000 281
355
429 WpwA N
/z->
0-
40
—P
50
96
100 150
— 191 |,
1 1 i 1 ' 11 *
200 . 250
—L
400
36.20 36.40 36.60 36.80
m/z 147.00 86.25%
Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7...
147 221
73
-----
5000
36.20 36.40 36.60 36.80
191 m/z 221.10 84.04%
117 279
45
—
249 1 ............ k
0- ■' i
m/z-> 50 100 150 200 250 . 300 350 400
Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime...
73 147
281 36.20 36.40 36.60 36.80
5000 m/z 280.95 47.56%
369
45
0- H 95 117
IP—— . 1 177.207 , 249, 1
, -| . . . " T77 Til [ I
310 ,341 ...
/z-> 50 100 150 200 250 300 350 400 Wwldlk
Abundance #87845: 2,6-Dimethyl-3,4-bis(trimethylsilyloxymethyl)pyridine 1 ’ 1 1 1 1 1 1 1 1 1 ■ • । ■ ■ ■ ■ । ■
Z!1 36.20 36.40 36.60 36.80
73
m/z 207.00 44.10%
5000 147 WlnpnWadsos
178
45
0
15 I. 1,"r"t
"I '
93120,
T 1 <■4 i-, 1 |h । h
266 296
m/z-> 50 100 150 200 250 300 350 400 36.20 36.40 36.60 36.80
11380.D 050102.M Mon May 20 15:46:53 2002 Page 14
NYC-WTC_000025123
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