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GCMS analysis results for sample AE11381, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.

NYC-WTC_000025102–000025126

Folder label: “GCMS X 5/15/02 A 5/17/02

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Scanned page image, NYC-WTC_000025121
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NYC 9/11 Public Portal Document Library aearen compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11380.D Vial: 7 Acq On : 17 May 2002 5:40 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ******************************************** * * * ********************** Peak Number 9 3,6-Dioxa-2,4,5,7-tetrasila ... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

34.36 0.24 ug/L 171748 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 43/ 2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 32 3 Malonic acid, 2-(2,3-dihydrobenz... 266 C13H1406 1000158-50-7/12 4 Benzene, l-fluoro-4-(2-cyanoethe... 147 C9H6FN 027530-50-3/10 Abundance Scan 5324 (34.361 min): 11380. D (-5317) (-) m/z 73.10 100:00% 73 147 221 5000 281 355 An MA 14 , 4AAM rAPr 96 191 429 34.00 34.20 34.40 34.60 44 — 0- I, ..................................... .................. m/z 147.00 76.65% 1 i Tl/Z-> 50 100 150 200 250 300 350 400 Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 2221

73 ............ ............. ............. 5000’ 34.00 34.20 34.40 34.60 191 m/z 221.10 57.31% 117 279 — 45 i I., 249 . / 01 TT 1 1 ' m/z—> 50 100 150 200 250 . 300 350 400 Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 73 147 281 34.00 34.20 34.40 34.60 5000 m/z 281.10 42.87%

45 369 0 H 1 95 117 ■ i I 177 297226 249 . 1 ■ 1 1 i ' ■ ■' r 1 i 310 341 . m/z-> 50 100 150 200 250 300 350 400 Abundance #66292: Malonic acid, 2-(2,3-dihydrobenzo[b]furan-5-yl)-2-... 1 147 34.00 34.20 34.40 34.60 m/z 207.00 40.36%

5000

91 207 pww/oakor/w 65 7 119 266 39 177 233 1 0 ' i ' *14 r > i ■ < ■ ■ i ■ ■ i ■ ■ ■ ■ i ■

m/z-> 50 100 150 200 250 300 350 400 34.00 34.20 34.40 34.60

11380.D 050102.M Mon May 20 15:46:52 2002 Page 12

NYC-WTC_000025121

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NYC-WTC_000025121Source: NYC Law Department, mirrored locally

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