GCMS analysis results, sample AE12534, June 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014578–000014606

Folder label: “GCMS X 5/28/02 A 5/29/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12534.D Vial: 25 Acq On : 30 May 2002 5:37 am Operator: McLean Sample. : gc/ms scan 5/28 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 20 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

39.23 0.36 ug/L 157964 Perylene-dl2 34.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 53 2 3-Benzofurancarboxylic acid, 2-[... 282 C17H14O4 040800-98-4/5 3 l-Aza-2-sila-5-boracyclopent-3-e ... 221 C12H24BNSi 081620-70-4 5 4 2(1H)-Quinolinone, 4-phenyl- 221 C15H11NO 005855-57-2 5 Abundance Scan 6153 (39.232 min): 12534.D (-6140) (-) m/ z 73.10 7100.00% 73 147 / 221

5000-

191 281 355 w:h Oh Hn 49 96 |l-. Jj ■ .dl i ■" ■ i “ " i “ " i ■1 ■ ■ i ■ ■ • • । I “ i • ■1 ■ I ■ > “ । “ • i ■ “ ‘ i" ■111 38.80 39.00 39.20 39.40 39.60 m/z 147.00 95.53% miz—> 20 40 60 80 100 120 140 160 180 2(X) 220 240 260 280 300 320 340 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 2211

73 5000- 38.80 39.00 39.20 39.40 39.60 191 m/z 221.10 79.15% 117 279

miz—> 28 45 0- | ■ ' ■ • ! ■ ■ • 101 ■ ■ < ■ | ■ ■ ■ ■ | ‘ 4 —74 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 [ 245 263 . 295 . 11... । ■... . .'f।।.... ।.... ।.... ।.

Abundance #87976:3-Benzofurancarboxylic acid, 2-[(2-hydroxyphenyl)m... 221 250 ' ' I ' ' 282 38.80 39.00 39.20 39.40 39.60 5000 m/z 355.00 24.79% 165 44 194 77 97 139 O-mmp- 1’II 112711-mmmmmmmTTTTT n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #87910:1-Aza-2-siIa-5-boracyclopent-3-ene, 4,5-diethyH.... 192 221 38.80 39.00 39.20 39.40 39.60 137 m/z 281.00 23.83%

5000 59 112 164 , 27 0— 444# 1 “ ‘ I" “ I ‘ ' I ‘ ' I ‘ ‘ I' ‘‘ I' “ • I ‘ /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 38.80 39.00 39.20 39.40 39.60

12534.D 052202.M Mon Jun 03 11:47:02 2002 Page 23

NYC-WTC_000014605

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000014605Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS sample analysis results, AE11903, June 3, 2002 · Box DEP Box 15

NYC-WTC_000012908

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997