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GCMS analysis results, sample AE12534, June 2002

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Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014578–000014606

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary , Operator ID: McLean Date Acquired: 30 May 2002 5:37 am ’ Data File: C:\MSDCHEM\l\DATA\052902\12534.D Name: gc/ms scan 5/28 Mise: Method: C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone Methylene Chloride 3.70 3.2 ug/L 2049400 1. 9.90 25279300 40.0 Acetic acid, chlo... 3.73 3.6 ug/L 2305880 1 9.90 25279300 40.0 2-Amino-oxazole 3.82 6.3 ug/L 4005870 1 9.90 25279300 40.0 O-Methylhydroxyla... 3.95 1.1 ug/L 693842 1 9.90 25279300 40.0 Crotonic acid 3.98 1.7 ug/L 1075750 1 9.90 25279300 40.0 Propiolonitrile 4.02 1.5 ug/L 932035 1 9.90 25279300 40.0 Methylene Chloride 4.30 1.0 ug/L 617667 1 9.90 25279300 40.0 2-Chloroethanol . 4.45 1.2 ug/L 758259 1 9.90 25279300 40.0 Propanoic acid. m. . 4.53 1.1 ug/L 707758 1 9.90 25279300 40.0 2-Pentanone, 4-hy... 5.95 0.8 ug/L 532083 1 9.90 25279300 40.0 Cyclopentasiloxan... 12.37 2.5 ug/L 2159630 2 13.39 34327300 40.0 1,5-Naphthalenedi... 22.53 0.2 ug/L 238781 4 22.91 38497300 40.0 Phenanthrene-dl0 23.06 0.3 ug/L 301464 4 22.91 38497300 40.0 Cyclononasiloxane... 33.19 0.7 ug/L 308728 6 34.65 17704700 40.0 Cyclononasiloxane... 34.31 1.2 ug/L 535753 6 34.65 17704700 40.0 Phenyl t-butyl te... 34.91 0.3 ug/L 149443 6 34.65 17704700 40.0 Cyclononasiloxane... 35.37 1.4 ug/L 614363 6 34.65 17704700 40.0 3,6-Dioxa-2,4,5,7... 36.43 1.3 ug/L 564858 6 34.65 17704700 40.0 3,6-Dioxa-2,4,5,7... 37.70 0.9 ug/L 378010 6 34.65 17704700 40.0 3,6-Dioxa-2,4,5,7. . . 39.23 0.4 ug/L 157964 6 34.65 17704700 40.0

12534.D 052202.M Mon Jun 03 11:47:02 2002 Page 24

NYC-WTC_000014606

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NYC-WTC_000014606Source: NYC Law Department, mirrored locally

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