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GCMS analysis report sample AE11908, June 4, 2002

Machine-extracted title · confidence 95%

GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.

NYC-WTC_000013014–000013042

Folder label: “GCMS X 5-21-02 A 5-22-02

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Scanned page image, NYC-WTC_000013042
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NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary

, Operator ID: Mclean Date Acquired: 23 May 2002 1:14 am Data File: C:\MSDCHEM\1\DATA\052202\11908.D Name: 5/21 ad Mise: Method: C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L *e

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone

Methylene Chloride 3.71 1.8 ug/L 1152960 1 9.90 24935700 40.0 Methylene Chloride 3.74 1.0 ug/L 630823 1 9.90 24935700 40.0 2-Butenal, 2-methyl- 3.76 0.6 ug/L 397925 1 9.90 24935700 40.0 2-Butenal, 3-methyl- 3.78 0.8 ug/L 508727 1 9.90 24935700 40.0 Oxazolidine, 3-me... 3.81 0.7 ug/L 433518 1 9.90 24935700 40.0 Ethyl Chloride 3.83 2.2 ug/L 1348470 1 9.90 24935700 40.0 2,2,6-Trimethyl-4... 3.90 1.8 ug/L 1111690 1 9.90 24935700 40.0 Methylene Chloride 4.00 1.2 ug/L 751370 1 9.90 24935700 40.0 Krypton 4.19 0.6 ug/L 380130 1 9.90 24935700 40.0 Toluene 4.27 1.2 ug/L 771358 1 9.90 24935700 40.0 2-Pentanone, 4-hy... 5.93 10.4 ug/L 6484920 1 9.90 24935700 40.0 Cyclopentasiloxan. .. 12.37 1.4 ug/L 1202730 2 13.39 33508900 40.0 1,5-Naphthalenedi... 22.54 0.3 ug/L 233616 4 22.91 36901200 40.0 1,1,1,5,7,7,7-Hep.. . 32.00 0.7 ug/L 421251 5 30.76 25446300 40.0 1,1,1,5,7,7,7-Hep. . . 33.20 2.3 ug/L 962060 6 34.66 16440500 40.0 Cyclononasiloxane ... 34.32 3.5 ug/L 1440790 6 34.66 16440500 40.0 Cyclononasiloxane. .. 35.38 4.0 ug/L 1626260 6 34.66 16440500 40.0 Cyclononasiloxane. .. 36.45 4.0 ug/L 1648480 6 34.66 16440500 40.0 Cyclononasiloxane. .. 37.71 2.6 ug/L 1053280 6 34.66 16440500 40.0 Cyclononasiloxane. .. 39.25 1.6 ug/L 661031 6 34.66 16440500 40.0

r

11908.D 052202.M Tue May 28 12:16:00 2002 Page 24

NYC-WTC_000013042

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NYC-WTC_000013042Source: NYC Law Department, mirrored locally

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