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GCMS blank analysis results, sample AE11799, May 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.

NYC-WTC_000012751–000012778

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Tentatively Identified Compound (LSC) summary .* Operator ID: Mclean Date Acquired: 22 May 2002 3:27 pm Data File: C:\MSDCHEM\1\DATA\052202\521LB.D Name: 5/21 ad Mise: Method: C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone Methylene Chloride 3.70 1.1 ug/L 710558 1 9.90 24873700 40.0 Propiolonitrile 3.73 0.8 ug/L 494472 1 9.90 24873700 40.0 Azetidine, 1-nitr... 3.75 2.5 ug/L 1545090 1 9.90 24873700 40.0 Carbonic chloride... 3.86 0.6 ug/L 388040 1 9.90 24873700 40.0 Methylene Chloride 3.89 0.7 ug/L 445502 1 9.90 24873700 40.0 2-Butyne-l,4-diol.. . 3.92 0.7 ug/L 407455 1 9.90 24873700 40.0 Methylene Chloride 3.96 0.9 ug/L 556932 1 9.90 24873700 40.0 Toluene 4.26 1.3 ug/L 829441 1 9.90 24873700 40.0 Dicyandiamide 4.44 0.5 ug/L 280925 1 9.90 24873700 40.0 2-Pentanone, 4-hy... 5.93 10.4 ug/L 6466930 1 9.90 24873700 40.0 Cyclopentasiloxan... 12.37 1.4 ug/L 1146130 2 13.39 33256100 40.0 Pyrazolo[1,5-a]py... 34.81 0.4 ug/L 176182 6 34.66 15981300 40.0 6-Bromoquinaldine 34.86 0.6 ug/L 226501 6 34.66 15981300 40.0 3,6-Dioxa-2,4,5,7.. . 34.95 0.5 ug/L 199921 6 34.66 15981300 40.0 (p-Methoxyphenyl)... 35.00 0.4 ug/L 169471 6 34.66 15981300 40.0 9H-Purin-6-amine,... 35.03 0.6 ug/L 233266 6 34.66 15981300 40.0 Heptasiloxane, 1,... 35.38 0.6 ug/L 227136 6 34.66 15981300 40.0 Tris (trimethylsil . . . 36.45 0.4 ug/L 175597 6 34.66 15981300 40.0 2,6-Dimethyl-3,4-... 37.72 0.4 ug/L 161972 6 34.66 15981300 40.0 l-Monolinoleoylgl... 39.25 0.4 ug/L 148480 6 34.66 15981300 40.0

521LB.D 052202.M Tue May 28 11:58:11 2002 Page 24

NYC-WTC_000012778

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NYC-WTC_000012778Source: NYC Law Department, mirrored locally

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