Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
NYC-WTC_000012751–000012778Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\ 1 \DATA\ 0 52 2 02 \ 5 21LB. D Vial: 3 Acq On : 22 May 2002 3:27 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 20 1-Monolinoleoylglycerol tri... Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T.
39.25 0.37 ug/L 148480 Perylene-d12 34.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethy... 498 C27H54O4Si2 054284-45-6 23 2 l-Aza-2-sila-5-boracyclopent-3-e... 221 C12H24BNSi 081620-70-4 9 3 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 9 4 2-Amino-4-(4-chloroanilino)-S-tr... 221 C9H8C1N5 000500-42-5 5 Abundance Scan 6156 (39.249 min): 521 LB.D (-6144) (-) m/z 221.10 100.00% 73 147 2.!1
5000 355
44 282 429 1 ■ i 1 ■ ■ ‘ i • 39.00 39.20 39.40 39.60 AL 0- ' ■ i ■ ■ ' ■ i ■ ■ ■ ■ 1 ■ ■ ■ ■ 1 m/z 147.10 84.20% niz-> 50 100 150 200 250 300 350 400 450 Abundance #27370:1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 39.00 39.20 39.40 39.60 34 103 m/z 73.10 83.46% 281
miz-> 0- l— 444444124/1.177+44 +-249.,4,205327 355, 317+429,483, 50 100 150 200 250 300 350 400 450 Abundance #87910:1-Aza-2-sila-5-boracyclopent-3-ene, 4,5-diethyl-1 ,... 192 221 137 39.00 39.20 39.40 39.60 5000 m/z 355.00 46.65% 59 112 83
0- 27 # . sk . L L 1l . . ... ■ ■ i ■ ■ ' ■ i ' ■ ‘ ■ i ' ■ ■ ■ i ■ ' ■ ■ l miz-> 50 100 150 200 250 300 350 400 450 Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,57,7... 1 ■ 11'11/•। >'।'11111' 147 2.11 39.00 39.20 39.40 39.60 m/z 282.00 35.13% 73 5000 191 117 279 0 • 45 •‘ I ’ ' 1.., +4 I 249..+, .................. . ■ ■ 1 ' 1 ‘ ■ 1 Tnndnnm m/z—> 60 100 150 200 250 300 350 400 450 39.00 39.20 39.40 39.60
521LB.D 052202.M Tue May 28 11:58:11 2002 Page 23
NYC-WTC_000012777
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NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015496
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on June 5, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013418
Quality control document showing GCMS blank results for multiple volatile organic compounds analyzed on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025054
Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000012749
Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
Filed in the same folder
NYC-WTC_000012779
Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
Filed in the same folder
NYC-WTC_000012783
Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
Filed in the same folder
NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
Filed in the same folder