Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
NYC-WTC_000012751–000012778Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\521LB.D Vial: 3 Acq On : 22 May 2002 3:27 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 2,6-Dimethyl-3,4-bis(trimet... Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 37.72 0.41 ug/L 161972 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2,6-Dimethyl-3,4-bis(trimethylsi... 311 C15H29NO2Si2 1000079-52-1 1 2 Benzo[b]selenophene-2-carbonitri... 221 C10H7NSe 037007-55-9 9 3 Benzo[b]selenophene-3-carbonitri... 221 C10H7NSe 037007-54-8/9 4 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-v 6 9 Abundance Scan 5895 (37.716 min): 521 LB.D (-5884) (-) m/z 221.10 104 .00% 73 147 2.11
5000 281 429 355 96
miz-> Abundance o1 44 ■' i 50 1 100 - 150 191 200 250 300 350 #87845: 2,6-Dimethyl-3,4-bis(trimethylsilyloxymethy!)pyridine 400 37.40 37.60 37.80 38.00 m/z 73.10 85.95%
221 73
5000 147 37.40 37.60 37.80 38.00 178 m/z 147.00 84.71 45 0- 15 ... kii ... 92 1201. r1nr 44 266 296 m/z-> 50 100 150 200 250 300 350 400 Abundance #87883: Benzo[b]selenophene-2-carbonitrile, 3-methyl- 221 • ■ i • . ■ ‘ j 140 37.40 37.60 37.80 38.00 5000 m/z 207.05 45.97%
. 117 npwwwrWWMWNwi nz-> 0- ’ 50 63 88 I it f i il 100 150 A194 1
200 250 300 350 400 Abundance #87882: Benzo[b]selenophene-3-carbonitrile, 2-methyl- 221 '37'40 37.60 37.80 38.00 ‘ 140 m/z 281.00 45.25 5000
0- 63 00 113 1 I s > । lli -4 1.......... .......... 194 ■ ‘ I ' 1 ■' 1 1 1 1 1 1 1 1 1 1 1 1 1 n/z—> 50 100 150 200 250 300 350 400 37.40 37.60 37.80 38.00
521LB.D 052202.M Tue May 28 11:58:11 2002 Page 22
NYC-WTC_000012776
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NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015496
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on June 5, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013418
Quality control document showing GCMS blank results for multiple volatile organic compounds analyzed on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025054
Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000012749
Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
Filed in the same folder
NYC-WTC_000012779
Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
Filed in the same folder
NYC-WTC_000012783
Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
Filed in the same folder
NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
Filed in the same folder