NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\052202\11903.D Vial: 10
Acq On : 22 May 2002 9:09 pm Operator: Mclean
Sample : 5/21 ad Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan "*
Library- : C:\DATABASE\NIST98.L
Peak Number 18 2,6-Dimethyl-3,4-bis(trimet... Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
36.45 1.32 ug/L 745171 Perylene-d12 34.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2,6-Dimethyl-3,4-bis(trimethylsi... 311 C15H29NO2Si2 1000079-52-1 5
2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 40
3 1,1,1,5,7,7,7-Heptamethy1-3,3-bi. . . 444 C13H40O5Si6 038147-00-1/40
4 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 38
Abundance Scan 5679 (36.447 min): 11903.D (-5668) (-) rn/z 73.10 100.00%
73 221
147
5000 281 355
w
429
51 325 36.20 36.40 36.60 36.80
191 „ I,
0- 1B
1
■ r ■ 1 1ih 1 PHT" ii ‘ ‘ ‘ ‘ I ‘ v ‘ ‘ I ‘ m/z 221.10 83.16%
vfz~> 50 100 150 200 250 300 350 400
Abundance #87845:2,6-Dimethyi-3,4-bis(trimethylsilyloxymethyl)pyridine
73 221
5000 147 —------4+4--
36.20 36.40 36.60 36.80
178 m/z 147.10 77.85%
45
niz->
0- 15 .
1 "1 -r rrttr
50
L 9-129 44,, 26.296.
100 150 400
200 250 300 350
Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7...
147 221
+444—4**A4a-4-——
21I
73 36.20 36.40 36.60 36.80
5000 m/z 280.95 39.22%
_
191
117 279
0-
45
1 ‘l , 1 ‘ f"1 1... L, 249 I............... •
miz-> 50 100 150 200 250 300 350 400
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)...
73 36.20 36.40 36.60 36.80
m/z 355.00 37.94%
147
5000 267
355 429
45 207
mfe->
0 /G
50 100 150 200 250 300 350 400
' 1 1 1 ■ *> I 1 1 1 1 1 1 1
36.20 36.40 36.60 36.80
11903.D 052202.M Tue May 28 12:08:00 2002 Page 21
NYC-WTC_000012933
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