GCMS analysis results for sample AE09335, May 2002

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Laboratory report documenting GCMS analysis of sample AE09335 conducted on May 8, 2002.

NYC-WTC_000044672–000044699

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9335.D Vial : 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 17 Cyclopent[e]-1,3-oxazine, o.. Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

38.50 0.47 ug/L 549541 Perylene-dl2 34.73

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopent[e]-1,3-oxazine, octahy... 216 C13H16N20 1000138-92-2 2 2 1-Cycloheptene-3-carboxamide, N-... 215 C14H17NO 1000159-24-4 14 3 2H-Pyran, 2-(7-heptadecynyloxy)t. . . 336 C22H40O2 056599-50- 10 4 Bisvertinol 498 C28H3408 1000145- -4 10 Abundance Scan 6028 (38.497 min): 9335.D (-6012) (-) m/z 81.10 100.00% 43 81 2 5 107 149

5000 233 401 i31 193 ' ' 1 1 ' 1 ' I 38.20 38.40 38.60 38.80 TT I 1' j 1 " । ‘ ‘' ।"111 p ' " i1 । i । ii । । । . . . . । । . i|t 1'1 . । । > । . । । । । । । । । । . । . । > । । । । m/z 215.20 92.01% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #86591: Cyclopent[e]-1,3-oxazine, octahydro-2-(phenylimino... 2 5

5000 ' 1 I ' ' ' 1 I ■ 1 i 1 1 1 135 38.20 38.40 38.60 38.80 41 Ju., 93 I m/z 43.15 89.79%

wwr | 65 ' I' ’111' '"I"' i" " i" " r ' I" ’ ’ I i ’ " ■ i " " i" " i " m/z-> 20 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #40480:1-Cycloheptene-3-carboxamide, N-phenyl- 90 215 ‘ 7I/" ... I .... I I ... ] >>> I 38.20 38.40 38.60 38.80 5000 m/z 55.10 87.13% 67 41

uL, ++ 1,9 148 172 TIT "TPL . | ... । | i i . । । । । . i j . i i । Uuv i J i i । । । i > i r । i TTTm pt/u/ m/z-> 20 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #13044: 2H-Pyran, 2-(7-heptadecynyloxy)tetrahydro- 55 38.20 38.40 38.60 38.80 81 m/z 57.10 77.07%

5000 29 121 147 | 175 — # 4 1 —44 .203231 —T—259 C I mump280 305 334 i11" i 11 'H1I‘1111 11 ' ■ | • I ■ r I | I I | | I I

/z-> 20 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 38.20 38.40 38.60 38.80

9335 .D 050102 .M Mon May 06 14:00:01 2002 Page 22

NYC-WTC_000044697

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