GCMS analysis results for sample AE10810, May 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\051402\10810.D Vial: 20 Acq On : 15 May 2002 5:50 am Operator: Mclean Sample : 5/7 kb Inst Instrumen Mise : Multiplr: 1.00 • MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Cyclohexane, (1-methylethyl)- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

35.69 0.91 ug/L 811759 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Cyclohexane, (1-methylethyl)- 126 C9H18 000696-29-7 12 2 1-Eicosyne 278 C20H38 000765-27-5 9 3 Oxirane, heptadecyl- 282 C19H380 067860-04-2 9 4 7-Azabicyclo[4.1.0]heptane, 1-me... 153 C10H19N 077774-31-3 9 Abundance Scan 5550 (35.689 min): 10810.D (-5546) (-) m/ z 82.10 100.00% 82

5000 43 67 96 113 208 281 TI ' ' W. 1 35.40 35.60 35.80 36.00 0- .... . 60p 80 100 120 140 160 180 200 220 ......... | m/ Z 83.05 49.00%

M m/z-> 20 40 240 260 280 Abundance #116331: Cyclohexane, (1-methylethyl)- 55 82

5000 41 MAMM.s.l,M“MM 35.40 35.60 35.80 36.00 126 m/ z 43.10 41.10%

/z-> O—TT 20 27 l . । !■ 40 60 L69 । 95 111 TtOdn—TT 80 100 120 140 160 180 200 220 240 260 280 Abundance #32343: 1-Eicosyne 43 82 96

57 35.40 35.60 35.80 36.00 5000 m/ z 67.20 28.78%

109 ,i 11 123 138 152166180194207 222 236 250263 277 01 ■ ■ । ■ r "IBBn,—um—nmuun/*mm—uTMTU m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #32326: Oxirane, heptadecyl- TTT ' ' T 1 1 ' ' I 43 82 35.40 35.60 35.80 36.00 96 m/ z 42.20 27.58% 57 5000 29 110

m/z-> 0 J H 1 ' i ' 11 1 T 44 — ah————7 1— I 124,29 I. j 152166180194208222236250 264 282 ।"" । "I । । 1" ।—। 1 i i f i H । H i i t ‘ i I । । — i । — i [ n > r 20 40 60 80 100 120 140 160 180 200 220 240 260 280 1... 35.40 35.60 35.80 36.00 I

10810.D 050102.M Thu May 16 12:39:57 2002 Page 20

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